期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 138, 期 9, 页码 2929-2932出版社
AMER CHEMICAL SOC
DOI: 10.1021/jacs.5b13038
关键词
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资金
- Canadian Foundation for Innovation (CFI)
- NSERC Discovery Grant
- FRQNT Nouveaux Chercheurs grant
- McGill University
- Ruder Bogkovic Institute
- Center of Excellence for Advanced Materials and Sensors, Croatia
- European Commission
- Croatian Ministry of Science, Education and Sports Marie Curie program NEWFELPRO [62]
Mechanochemistry provides a rapid, efficient route to metal organic framework Zn-MOF-74 directly from a metal oxide and without bulk solvent. In situ synchrotron X-ray diffraction monitoring of the reaction course reveals two new phases and an unusual stepwise process in which a close-packed intermediate reacts to form the open framework. The reaction can be performed on a gram scale to yield a highly porous material after activation.
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