期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 138, 期 32, 页码 10116-10119出版社
AMER CHEMICAL SOC
DOI: 10.1021/jacs.6b06394
关键词
-
资金
- European Research Council [671093]
- Spanish Government [MAT2015-71842-P, MAT2012-38567-C02-01, SEV-2012-0267]
- Generalitat Valenciana
- Italian project FIR Exploring the Nanoworld
- European Research Council (ERC) [671093] Funding Source: European Research Council (ERC)
In this work a new ultrafast data collection strategy for electron diffraction tomography is presented that allows reducing data acquisition tithe by one order of Magnitude.,,This Methodology minimizes the radiation damage of, beam-sensitive materials, such as microporous materials. This method, combined with the precession of the electron beam, provides high quality data enabling the determination of very complex structures. Most importantly,, the implementation of this new, electron diffraction methodology is, easily affordable in any modem electron Microscope. As a proof of concept, we have solved a new highly complex zeolitic structure named ITQ-58, with a very low symmetry (triclinic) and a large unit cell volume (1874.61(3)), containing 16 silicon and 32 oxygen atoms in its asymmetric unit, which would be very difficult to solve with the state of the art techniques.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据