4.7 Article

Microstructural characterization and mechanical properties of (TiB ? TiC) reinforced Ti-6Al-4V prepared by melt hydrogenation

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DOI: 10.1016/j.jmrt.2023.01.094

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Microstructural characterization; Titanium matrix composites; Melt hydrogenation; Nano-hardness

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TiB and TiC reinforced Ti-6Al-4V matrix composites were prepared using melt hydrogenation, with a total fraction of reinforcements at 5 vol % and a ratio of TiB to TiC at 1:1. The study investigated the effects of melt hydrogenation on the solidification process, phase composition, and microstructure of the titanium matrix, and observed the morphology and distribution of reinforcements with and without hydrogen. Nano-hardness measurements were also carried out. The results showed that melt hydrogenation can alter the solidification process, increase the b phase, and refine the lamellar structure. Hydrogen resulted in larger reinforcements that aggregated at the grain boundary, forming a network structure. Nano-hardness was slightly reduced by hydrogen for both the titanium alloy and the reinforcements. In summary, melt hydrogenation can maintain or slightly reduce the strength of the composites at room temperature and decrease the nano-hardness.
TiB and TiC reinforced Ti-6Al-4V matrix composites were prepared by melt hydrogena-tion, in which the total fraction of the reinforcements was 5 vol % and the ratio of TiB to TiC was 1:1. The effects of melt hydrogenation on the solidification process, phase composi-tion, and microstructure of the titanium matrix were studied. The morphology and dis-tribution of the reinforcement without and with hydrogen were observed. Moreover, the nano-hardness of the composites was measured. The results show that the solidification process of the matrix can be changed by melt hydrogenation, which resulting the increase of b phase and refining of a lamellar in titanium alloy. Hydrogen increased the size of the reinforcements, which aggregated at the grain boundary of the primary b phase and formed a network structure. Hydrogen reduced the nano-hardness both of the titanium alloy and the reinforcements slightly. In summary, melt hydrogenation can maintain or slightly reduce the strength of the composites at room temperature and decrease the nano -hardness.(c) 2023 Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

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