4.6 Article

Preparation of graphitized carbon by the corn straw liquefaction method

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RSC ADVANCES
卷 13, 期 5, 页码 2984-2992

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ROYAL SOC CHEMISTRY
DOI: 10.1039/d2ra07352h

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Corn straw-based graphitized carbon was synthesized using carbonization and catalyzed graphitization with corn straw as the raw material and catalytic liquefaction technology. A mixture of polyethylene glycol (PEG200) and glycerol in a mass ratio of 7:3 was used as the liquefied agent, and hydroxydiethylidene glycolic acid was employed as the liquefied catalyst. The graphitized carbon exhibited improved graphitization, a lamellar microstructure, and reduced defects when carbonized at 600 degrees C, graphitized at 850 degrees C, and using ferric acetylacetonate as the catalyst at a concentration of 7.0 mmol g(-1). The yield of corn straw-based graphitized carbon reached 22.20%.
Corn straw-based graphitized carbon was prepared by carbonization and a catalyzed graphitization method using corn straw as the raw material and catalytic liquefaction technology. A mixture of polyethylene glycol (PEG200) compounded with glycerol in the mass ratio of 7 : 3 was used as the liquefied agent, meanwhile 0.3 g of hydroxydiethylidene glycolic acid acted as the liquefied catalyst. The liquefied products were treated via carbonization and graphitization processes to form graphitized carbon. The graphitized carbon showed better graphitization, a microscopic lamellar structure, and smaller defects, when the carbonized temperature was 600 degrees C, graphitization temperature 850 degrees C, and the catalyst was ferric acetylacetonate at a concentration of 7.0 mmol g(-1). The corn straw-based graphitized carbon yield reached 22.20%.

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