4.6 Article

SiOC Screens with Aligned and Adjustable Pore Structure for Screen Channel Liquid Acquisition Device

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MATERIALS
卷 16, 期 3, 页码 -

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MDPI
DOI: 10.3390/ma16031063

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SiOC screens; unidirectional freeze-casting; bubble point; polymer-derived ceramic; gas-liquid phase separation

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The development of porous ceramic screens with high chemical stability, low density, and thermal conductivity has the potential to become promising screen channel liquid acquisition devices (SC-LADs) for propellant management under microgravity conditions in the future. SiOC screens with aligned pores were fabricated using freeze-casting and applied as a SC-LAD. The pore window sizes and open porosity varied depending on the freezing temperature and the solid loading. The SC-LADs demonstrated high liquid removal capabilities but with variations in pressure drop and bubble ingestion, depending on the open porosity and pore window sizes of the screens.
The development of porous ceramic screens with high chemical stability, low density, and thermal conductivity can lead to promising screen channel liquid acquisition devices (SC-LADs) for propellant management under microgravity conditions in the future. Therefore, SiOC screens with aligned pores were fabricated via freeze-casting and applied as a SC-LAD. The pore window sizes and open porosity varied from 6 mu m to 43 mu m and 65% or 79%, depending on the freezing temperature or the solid loading, respectively. The pore window size distributions and bubble point tests indicate crack-free screens. On the one hand, SC-LADs with an open porosity of 79% removed gas-free liquid up to a volumetric flow rate of 4 mL s(-1). On the other hand, SC-LADs with an open porosity of 65% were limited to 2 mL s(-1) as the pressure drop across these screens was relatively higher. SC-LADs with the same open porosity but smaller pore window sizes showed a higher pressure drop across the screen and bubble ingestion at higher values of effective screen area when increasing the applied removal volumetric flow rate. The removed liquid from the SC-LADs was particle-free, thus representing a potential for applications in a harsh chemical environment or broad-range temperatures.

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