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The crystal structure of tris(carbonyl)-bis(carbonyl)-[μ-propane-1,2-dithiolato]-(benzyldiphenylphosphine)diiron (Fe-Fe), C27H23Fe2O5PS2

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WALTER DE GRUYTER GMBH
DOI: 10.1515/ncrs-2022-0520

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A C27H23Fe2O5PS2 crystal was discovered in this experiment. It belongs to the monoclinic system and P2(1)/c space group. The cell parameters were determined as a = 11.3170 angstrom, b = 16.1774 angstrom, c = 15.2170 angstrom, β = 92.933(1)degrees. The volume of the cell was 2782.3(2) angstrom(3) with 4 formula units. The structure quality indicators R-gt(F) = 0.0537 and wR(ref)(F (2)) = 0.1636 were obtained at the temperature of 296(2) K.
C27H23Fe2O5PS2, monoclinic, P2(1)/c (no. 14), a = 11.3170(5) angstrom, b = 16.1774(8) angstrom, c = 15.2170(7) angstrom, beta = 92.933(1)degrees, V = 2782.3(2) angstrom(3), Z = 4, R-gt(F) = 0.0537, wR(ref)(F (2)) = 0.1636, T = 296(2) K.

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