期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 81, 期 6, 页码 2252-2260出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b02579
关键词
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资金
- National Natural Science Foundation of China [21302109, 21302110, 21375075]
- Taishan Scholar Foundation of Shandong Province
- Natural Science Foundation of Shandong Province [ZR2015JL004]
A direct difunctionalization protocol of alkenes with nitriles and thiols toward beta-acetamido sulfide derivatives has been proposed under metal-free synthesis conditions. The present protocol provides the facile and highly efficient synthesis of various beta-acetamido sulfides in a scaled-up manner with good to excellent yields simply using inexpensive molecular iodine as a catalyst, DMSO as a mild oxidant, and readily available thiols as thiolating reagents.
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