期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 81, 期 15, 页码 6795-6799出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.6b01005
关键词
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资金
- EPSRC
- University of Bath
- EPSRC Doctoral Training Centre in Sustainable Chemical Technologies [EP/G03768X/1]
A practically simple derivatization protocol for determining the enantiopurity of chiral diols by H-1 NMR spectroscopic analysis is described. Diols were treated with 0.5 equiv of 1,3-phenyldiboronic acid to afford mixtures of diastereomeric boronate esters whose homochiral/heterochiral ratios are an accurate reflection of the diol's enantiopurity.
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