期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 81, 期 5, 页码 1850-1857出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.5b02614
关键词
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资金
- Agence Nationale de la Recherche [ANR-13-BSV8-0020]
- Universite Paris-Sud
- French Ministry of Superior Education and Research
- CNRS
- LabEx LERMIT
- Agence Nationale de la Recherche (ANR) [ANR-13-BSV8-0020] Funding Source: Agence Nationale de la Recherche (ANR)
A straightforward palladium-catalyzed oxidative hydroxylation of azobenzenes is reported. The developed methodology tolerates various functional groups and allows the synthesis of diverse unsymmetrical azophenols under mild conditions in good to excellent yields. A complementary procedure was also investigated by in situ generation of PIFA. This study represents the first general method for the synthesis of o-hydroxyazobenzenes starting from simple azoarenes.
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