期刊
JOURNAL OF NUCLEAR MATERIALS
卷 473, 期 -, 页码 264-271出版社
ELSEVIER
DOI: 10.1016/j.jnucmat.2016.01.041
关键词
-
资金
- U.S. Department of Energy by Lawrence Livermore National Laboratory [DE-AC52-07NA27344]
- U.S. Department of Homeland Security, Domestic Nuclear Detection Office
Nuclear forensics requires accurate quantification of discriminating microstructural characteristics of the bulk nuclear material to identify its process history and provenance. Conventional metallographic preparation techniques for bulk plutonium (Pu) and uranium (U) metals are limited to providing information in two-dimension (2D) and do not allow for obtaining depth profile of the material. In this contribution, use of dual-beam focused ion-beam/scanning electron microscopy (FIB-SEM) to investigate the internal microstructure of bulk Pu and U metals is demonstrated. Our results demonstrate that the dual-beam methodology optimally elucidate microstructural features without preparation artifacts, and the three-dimensional (3D) characterization of inner microstructures can reveal salient microstructural features that cannot be observed from conventional metallographic techniques. Examples are shown to demonstrate the benefit of FIB-SEM in improving microstructural characterization of microscopic inclusions, particularly with respect to nuclear forensics. (C) 2016 Elsevier B.V. All rights reserved.
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