Crystalline phosphides/amorphous oxides composite for energy-saving hydrogen production assisted by efficient urea oxidation reaction

Article Chemistry, Physical

The polyoxometalates mediated preparation of phosphate-modified NiMoO4_x with abundant O-vacancies for H2 production via urea electrolysis

Yunfeng Qiu et al.

Summary: This study develops a facile and large-scale method to prepare bifunctional HER and UOR electrocatalysts for H-2 production via urea electrolysis in a less-energy saving way.

JOURNAL OF COLLOID AND INTERFACE SCIENCE (2023)

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Article Chemistry, Multidisciplinary

Dense Crystalline-Amorphous Interfacial Sites for Enhanced Electrocatalytic Oxygen Evolution

Dan Li et al.

Summary: The synchronous dual-phase synthesis of crystalline Ag and amorphous NiCoMo oxides on nickel foam resulted in a highly efficient and stable OER electrocatalyst. The dense c-a interfacial sites effectively modulate the electronic structure of the interfacial sites and promote phase transition, enhancing catalytic performance.

ADVANCED FUNCTIONAL MATERIALS (2022)

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Article Chemistry, Multidisciplinary

Crystalline-Amorphous Interfaces Coupling of CoSe2/CoP with Optimized d-Band Center and Boosted Electrocatalytic Hydrogen Evolution

Shijie Shen et al.

Summary: This study achieves deep optimization of catalytic activity by constructing a crystalline-amorphous CoSe2/CoP heterojunction, optimizing the valence state and H adsorption of Co, and lowering the kinetic barrier of the hydrogen evolution reaction. The heterojunction shows competitive properties in acidic, neutral, and basic media.

ADVANCED MATERIALS (2022)

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Article Chemistry, Multidisciplinary

Fluorine Engineered Self-Supported Ultrathin 2D Nickel Hydroxide Nanosheets as Highly Robust and Stable Bifunctional Electrocatalysts for Oxygen Evolution and Urea Oxidation Reactions

Swati J. Patil et al.

Summary: In the field of electrocatalytic water splitting, developing efficient noble-metal-free electrocatalysts remains a challenge. A scalable one-step synthesis approach was used to prepare self-supported fluorine-modified 2D ultrathin nickel hydroxide nanosheets, which demonstrated enhanced redox activity, electrical conductivity, and a large number of exposed active sites for improved charge migration during electrocatalytic reactions.

SMALL (2022)

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Article Chemistry, Physical

Hierarchical Structure of CuO Nanowires Decorated with Ni(OH)2 Supported on Cu Foam for Hydrogen Production via Urea Electrocatalysis

Hainan Sun et al.

Summary: By constructing a hierarchical structure of CuO nanowires decorated with nickel hydroxide on 3D Cu foam, this research achieved a significant reduction in the potential of urea oxidation reaction to 1.334 V, along with enhanced activity up to 100 mA cm(-2), and exceptional stability. Electrolysis of urea using this developed electrocatalyst as the anode showed promising results in terms of energy-saving hydrogen production.

SMALL METHODS (2022)

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Article Energy & Fuels

Three-dimensional crystalline-Ni5P4@amorphous-NiOx core-shell nanosheets as bifunctional electrode for urea electro-oxidation and hydrogen evolution

Zhihui Ma et al.

Summary: In this study, we report the growth of Ni5P4 nanosheets on nickel foam as a bifunctional electrode for urea electrolysis. The electrode exhibits a unique crystalline@amorphous core-shell structure, which leads to outstanding urea oxidation performance. The electrode is superhydrophilic and aerophobic, facilitating the release of gas bubbles and preventing blockage of active sites. The electrode also shows excellent stability in both urea electrolysis and hydrogen evolution reactions.

FUEL (2022)

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Article Chemistry, Physical

Hydrogen Evolution Linked to Selective Oxidation of Glycerol over CoMoO4-A Theoretically Predicted Catalyst

Xiaowen Yu et al.

Summary: This study demonstrates the effectiveness of CoMoO4 catalyst for glycerol oxidation reaction, with high selectivity and efficiency, enabling the production of value-added products and high-purity hydrogen.

ADVANCED ENERGY MATERIALS (2022)

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Article Chemistry, Applied

High valence state of Ni and Mo synergism in NiS2-MoS2 hetero-nanorods catalyst with layered surface structure for urea electrocatalysis

Shuli Wang et al.

Summary: The study demonstrated the formation of high active state of Ni3+ induced by Mo6+ and their efficient synergism in NiS2-MoS2 hetero-nanorods powder catalyst, providing a new perspective for urea-assisted water electrolysis.

JOURNAL OF ENERGY CHEMISTRY (2022)

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Article Engineering, Environmental

Interface engineering of S-doped Co2P@Ni2P core-shell heterostructures for efficient and energy-saving water splitting

Wenzhi Yuan et al.

Summary: The ion-exchange strategy to fabricate cobalt phosphide nanowire decorated with nickel phosphide nanosheets core@shell heterostructured arrays with sulfur doping at the interface (S-Co2P@Ni2P) has been demonstrated to be effective for both hydrogen evolution reaction (HER) and urea oxidation reaction (UOR), showing optimized absorption/desorption energies of reactants/products to accelerate the catalytic kinetics of HER and UOR.

CHEMICAL ENGINEERING JOURNAL (2022)

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Article Chemistry, Multidisciplinary

Tunable d-Band Centers of Ni5P4 Ultra-Thin Nanosheets for Highly-Efficient Hydrogen Evolution Reaction

Chengcheng Miao et al.

Summary: By simple heteroatom doping, the d-band center position of ultra-thin 2D Ni5P4 nanosheets can be manipulated, leading to efficient hydrogen evolution reaction (HER). Proper Co doping achieves the best electrocatalytic performance with excellent stability.

ADVANCED MATERIALS INTERFACES (2022)

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Article Chemistry, Multidisciplinary

Identification and manipulation of dynamic active site deficiency-induced competing reactions in electrocatalytic oxidation processes

Runjia Lin et al.

Summary: This study investigates the competition between electrocatalytic organic compound oxidation reactions (OCORs) and oxygen evolution reaction (OER) using NiWO4-catalysed urea oxidation reaction (UOR) as an example. The competition is attributed to insufficient surface concentration of dynamic Ni3+. To address this issue, a controllable reconstruction of pseudo-crystalline bimetal oxides design strategy is proposed, resulting in an optimised electrocatalyst with significantly improved performance in alkaline urea electrolysis.

ENERGY & ENVIRONMENTAL SCIENCE (2022)

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Review Chemistry, Multidisciplinary

Electrocatalytic Hydrogen Production Trilogy

Yan Li et al.

Summary: The article summarizes recent advances in electrocatalytic hydrogen production, including traditional OER electron donation, sacrificial agent oxidation electron donation, and electrosynthesis reaction electron donation in three stages, and discusses related challenges and prospects.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

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Article Nanoscience & Nanotechnology

Coaxial Ni-S@N-Doped Carbon Nanofibers Derived Hierarchical Electrodes for Efficient H2 Production via Urea Electrolysis

Yongxia Zhang et al.

Summary: Electrochemical water splitting for hydrogen production is a promising strategy powered by solar energy. Hybrid water electrolyzers with Ni/Ni3S2@N-doped nanofibers have shown superior performance in urea electrolysis, achieving lower cell voltage and better stability compared to traditional water electrolyzers. The modulation of compositions and hierarchical nanostructure is effective in preparing efficient catalysts for H2 production via urea electrolysis, providing fast electrocatalytic kinetics.

ACS APPLIED MATERIALS & INTERFACES (2021)

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Article Chemistry, Multidisciplinary

Unveiling the Electrooxidation of Urea: Intramolecular Coupling of the N-N Bond

Wei Chen et al.

Summary: This study delves into the crucial role of nitrogenous nucleophile electrooxidation reaction (NOR) in the degradation and transformation of available nitrogen, particularly focusing on the transformation mechanism mediated by the beta-Ni(OH)(2) electrode. The study proposes the role of proton-coupled electron transfer (PCET) in bridging the electrocatalytic dehydrogenation and spontaneous nucleophile dehydrogenative oxidation reaction, with a specific focus on the urea oxidation reaction (UOR). Through both operando tracing and theoretical calculations, a mechanism for UOR involving intramolecular coupling of the N-N bond, accompanied by PCET, hydration, and rearrangement processes, is proposed to achieve high performance and approximately 100% N-2 selectivity. These findings shed light on the evolution of nitrogenous molecules during NOR, as well as fundamental aspects of electrocatalysis involving nitrogen-containing species.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

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Article Engineering, Environmental

Bimetallic Ni-Co@hexacyano nano-frameworks anchored on carbon nanotubes for highly efficient overall water splitting and urea decontamination

Supriya A. Patil et al.

Summary: The study successfully synthesized self-standing nanocuboids anchored on carbon nanotubes via an ion-exchange strategy, exhibiting excellent overall water-splitting and urea oxidation performance.

CHEMICAL ENGINEERING JOURNAL (2021)

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Article Engineering, Environmental

Modulation of the crystalline/amorphous interface engineering on Ni-P-O-based catalysts for boosting urea electrolysis at large current densities

Xiujuan Xu et al.

Summary: The study developed nickel-phosphorus-oxygen-based micro-nanostructures through a simple electrodeposition strategy, where NiO-NiPi exhibited significant anodic catalytic activity and NiP/NiO-NiPi showed faster cathodic hydrogen generation rate. The tunable catalytic activities were correlated with the interface structure and composition, aiding in enhancing electron transfer rates and increasing active site density.

CHEMICAL ENGINEERING JOURNAL (2021)

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Article Multidisciplinary Sciences

Isolated copper single sites for high-performance electroreduction of carbon monoxide to multicarbon products

Haihong Bao et al.

Summary: Electrochemical carbon monoxide reduction is a promising strategy for producing high-value multicarbon compounds, but low selectivities and Faradaic efficiencies are common. In this study, a single-atom copper catalyst supported on MXene showed high performance and stability in CO reduction.

NATURE COMMUNICATIONS (2021)

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Article Chemistry, Multidisciplinary

Regulating the Local Charge Distribution of Ni Active Sites for the Urea Oxidation Reaction

Liping Wang et al.

Summary: A tungsten-doped nickel catalyst (Ni-WOx) was developed with superior activity towards the urea oxidation reaction, accelerating the reaction kinetics and increasing the turnover frequency. Experimental results demonstrated that tungsten doping led to the formation of Ni3+ sites with superior activity, facilitating the catalytic reaction.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

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Article Chemistry, Physical

Ultrathin NiMn-LDH nanosheet structured electrocatalyst for enhanced electrocatalytic urea oxidation

Guoqiang Liu et al.

Summary: A study reported the successful assembly of an energy-saving water splitting system using ultrathin NiMn-LDH/CFC grown on commercial carbon fiber cloth, showing reliable electrocatalytic activities.

APPLIED CATALYSIS A-GENERAL (2021)

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Article Chemistry, Multidisciplinary

Oxygen-Incorporated NiMoP Nanotube Arrays as Efficient Bifunctional Electrocatalysts For Urea-Assisted Energy-Saving Hydrogen Production in Alkaline Electrolyte

Hao Jiang et al.

Summary: By synthesizing oxygen-incorporated nickel molybdenum phosphide nanotube arrays, this study successfully developed self-supporting O-NiMoP/NF electrodes with highly efficient bifunctional catalytic activity towards HER and UOR.

ADVANCED FUNCTIONAL MATERIALS (2021)

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Article Chemistry, Multidisciplinary

Deciphering and Suppressing Over-Oxidized Nitrogen in Nickel-Catalyzed Urea Electrolysis

Jianan Li et al.

Summary: Urea electrolysis is a promising technology for simultaneous H-2 production and nitrogen suppression in water energy production. However, prevalent nickel-based catalysts may over-oxidize urea into NO2- products, posing potential environmental hazards. Through experiments and calculations, a nitrogen-fate network was derived, leading to the development of a polyaniline-coating strategy to increase N-2 production. These findings offer insights into nitrogen fate in water-energy systems.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

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Article Chemistry, Multidisciplinary

Understanding the Roles of Electrogenerated Co3+ and Co4+ in Selectivity-Tuned 5-Hydroxymethylfurfural Oxidation

Xiaohui Deng et al.

Summary: The study demonstrates that Co3+ and Co4+ species in Co-based electrocatalyst play distinct roles in the electrochemical oxidation of 5-hydroxymethylfurfural (HMF), with Co4+ being crucial for the initial oxidation of hydroxyl groups. By tuning the applied potential, selective production of 5-hydroxymethyl-2-furancarboxylic acid and 2,5-furandicarboxylic acid can be achieved. This work provides essential mechanistic insights for Co-catalyzed organic oxidation reactions and may guide the design of more efficient electrocatalysts.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

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Article Chemistry, Physical

Constructing a Graphene-Encapsulated Amorphous/Crystalline Heterophase NiFe Alloy by Microwave Thermal Shock for Boosting the Oxygen Evolution Reaction

Zhichao Gong et al.

Summary: Efficient and robust catalysts for the oxygen evolution reaction (OER) are crucial for energy conversion technologies, with the core-shell electrocatalyst developed in this study showing significantly enhanced OER performance. The amorphous/crystalline structure of the NiFe alloy and graphene coatings played key roles in providing enriched active sites and electron transport pathways, leading to superior OER activity in 1 M KOH. This work provides insights for constructing metastable amorphous/crystalline heterophase catalysts for highly efficient electrocatalysis.

ACS CATALYSIS (2021)

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Review Chemistry, Physical

Progress and Perspectives in Photo- and Electrochemical-Oxidation of Biomass for Sustainable Chemicals and Hydrogen Production

Hui Luo et al.

Summary: Biomass is a recognized ideal resource substitute for fossil fuels, with oxidation derivatives from biomass-derived compounds being used in the production of biodegradable polymers and pharmaceuticals. Combining biomass oxidation with hydrogen generation reactions presents a promising strategy for coproducing high value chemicals and hydrogen.

ADVANCED ENERGY MATERIALS (2021)

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Article Energy & Fuels

Nickel ferrocyanide as a high-performance urea oxidation electrocatalyst

Shi-Kui Geng et al.

Summary: Researchers have found that the nickel ferrocyanide catalyst can drive the urea oxidation reaction with higher activity and stability. Moreover, the catalyst appears to operate via a different pathway, which facilitates the efficiency of ammonia production.

NATURE ENERGY (2021)

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Article Chemistry, Multidisciplinary

Discovering ultrahigh loading of single-metal-atoms via surface tensile-strain for unprecedented urea electrolysis

Ashwani Kumar et al.

Summary: Recent research has shown that incorporating tensile strain on the surface of a Co3O4 support can significantly inhibit the migration tendency of single-atom Rh, stabilizing a higher loading of Rh sites. This enhanced SAC, Rh-SA-S-Co3O4, exhibited exceptional pH-universal urea oxidation reaction activity and demonstrated robust stability in alkaline media, providing a general methodology towards high-loading single-atom catalysts for scalable applications.

ENERGY & ENVIRONMENTAL SCIENCE (2021)

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Article Chemistry, Physical

3D self-supported porous vanadium-doped nickel nitride nanosheet arrays as efficient bifunctional electrocatalysts for urea electrolysis

Rui-Qing Li et al.

Summary: In this study, V-doped Ni3N nanosheets arrays grown on nickel foam were developed as a bifunctional electrocatalyst for hydrogen evolution reaction (HER) and urea oxidation reaction (UOR). The catalyst exhibited excellent catalytic performances with low energy consumption and remarkable stability, making it promising for applications in energy-saving H-2 production and urea-related waste water treatment.

JOURNAL OF MATERIALS CHEMISTRY A (2021)

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Article Chemistry, Multidisciplinary

Ni2P nanoflakes for the high-performing urea oxidation reaction: linking active sites to a UOR mechanism

Haipeng Liu et al.

Summary: Urea electrolysis is an effective method for energy and environment issues, and Ni2P nanoflakes have been successfully synthesized as a catalyst for urea oxidation reaction (UOR), showing comparable activity to state-of-the-art catalysts. The in situ generation of NiOOH on Ni2P nanoflakes accelerates the UOR process, providing insights into the mechanism and new opportunities for designing low-cost Ni-based phosphide UOR catalysts.

NANOSCALE (2021)

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Article Chemistry, Multidisciplinary

Bimetal Schottky Heterojunction Boosting Energy-Saving Hydrogen Production from Alkaline Water via Urea Electrocatalysis

Chao Wang et al.

ADVANCED FUNCTIONAL MATERIALS (2020)

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Article Chemistry, Physical

Ni-Ni3P nanoparticles embedded into N, P-doped carbon on 3D graphene frameworks via in situ phosphatization of saccharomycetes with multifunctional electrodes for electrocatalytic hydrogen production and anodic degradation

Guixiang Li et al.

APPLIED CATALYSIS B-ENVIRONMENTAL (2020)

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Article Engineering, Environmental

In situ grown 3D hierarchical MnCo2O4.5@Ni(OH)2 nanosheet arrays on Ni foam for efficient electrocatalytic urea oxidation

Linna Sha et al.

CHEMICAL ENGINEERING JOURNAL (2020)

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Review Chemistry, Multidisciplinary

Designing Advanced Catalysts for Energy Conversion Based on Urea Oxidation Reaction

Bingjun Zhu et al.

SMALL (2020)

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Article Chemistry, Multidisciplinary

Metal-Organic Framework-Derived Co2P Nanoparticle/Multi-Doped Porous Carbon as a Trifunctional Electrocatalyst

Haitao Liu et al.

ADVANCED MATERIALS (2020)

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Article Chemistry, Multidisciplinary

2D Intrinsic Ferromagnetic MnP Single Crystals

Xian Sun et al.

SMALL (2020)

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Article Chemistry, Multidisciplinary

Ni, Co hydroxide triggers electrocatalytic production of high-purity benzoic acid over 400 mA cm-2

Hongling Huang et al.

ENERGY & ENVIRONMENTAL SCIENCE (2020)

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Article Chemistry, Physical

Efficient synergism of NiSe2 nanoparticle/NiO nanosheet for energy-relevant water and urea electrocatalysis

Zong Liu et al.

APPLIED CATALYSIS B-ENVIRONMENTAL (2020)

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Article Electrochemistry

Ni/NiO nanosheets for alkaline hydrogen evolution reaction: In situ electrochemical-Raman study

Alaa Y. Faid et al.

ELECTROCHIMICA ACTA (2020)

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Review Green & Sustainable Science & Technology

Direct Urea Fuel Cells: Recent Progress and Critical Challenges of Urea Oxidation Electrocatalysis

Georgepeter Gnana Kumar et al.

ADVANCED ENERGY AND SUSTAINABILITY RESEARCH (2020)

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Article Engineering, Environmental

Rational design of NiCo2S4 nanowire arrays on nickle foam as highly efficient and durable electrocatalysts toward urea electrooxidation

Linna Sha et al.

CHEMICAL ENGINEERING JOURNAL (2019)

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Article Chemistry, Multidisciplinary

Fe3C-Co Nanoparticles Encapsulated in a Hierarchical Structure of N-Doped Carbon as a Multifunctional Electrocatalyst for ORR, OER, and HER

Chun Cheng Yang et al.

ADVANCED FUNCTIONAL MATERIALS (2019)

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Article Chemistry, Multidisciplinary

Negative Charging of Transition-Metal Phosphides via Strong Electronic Coupling for Destabilization of Alkaline Water

Bo You et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2019)

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Article Chemistry, Multidisciplinary

A Lattice-Oxygen-Involved Reaction Pathway to Boost Urea Oxidation

Longsheng Zhang et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2019)

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Article Chemistry, Multidisciplinary

Identification of Key Reversible Intermediates in Self-Reconstructed Nickel-Based Hybrid Electrocatalysts for Oxygen Evolution

Jianwen Huang et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2019)

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Article Multidisciplinary Sciences

Nickel-molybdenum nitride nanoplate electrocatalysts for concurrent electrolytic hydrogen and formate productions

Yan Li et al.

NATURE COMMUNICATIONS (2019)

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Article Chemistry, Multidisciplinary

Homologous CoP/NiCoP Heterostructure on N-Doped Carbon for Highly Efficient and pH-Universal Hydrogen Evolution Electrocatalysis

Ramireddy Boppella et al.

ADVANCED FUNCTIONAL MATERIALS (2019)

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Article Materials Science, Multidisciplinary

Constructing Hierarchical Wire-on-Sheet Nanoarrays in Phase-Regulated Cerium-Doped Nickel Hydroxide for Promoted Urea Electro-oxidation

Junfeng Xie et al.

ACS MATERIALS LETTERS (2019)

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Article Chemistry, Multidisciplinary

Advantageous crystalline-amorphous phase boundary for enhanced electrochemical water oxidation

HyukSu Han et al.

ENERGY & ENVIRONMENTAL SCIENCE (2019)

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Article Chemistry, Physical

Tungsten-doped Ni-Co phosphides with multiple catalytic sites as efficient electrocatalysts for overall water splitting

Shan-Shan Lu et al.

JOURNAL OF MATERIALS CHEMISTRY A (2019)

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Article Chemistry, Multidisciplinary

Hierarchical CoP/Ni5P4/CoP microsheet arrays as a robust pH-universal electrocatalyst for efficient hydrogen generation

Ishwar Kumar Mishra et al.

ENERGY & ENVIRONMENTAL SCIENCE (2018)

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Article Chemistry, Physical

Local Charge Distribution Engineered by Schottky Heterojunctions toward Urea Electrolysis

Caicai Li et al.

ADVANCED ENERGY MATERIALS (2018)

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Article Chemistry, Multidisciplinary

A Janus Nickel Cobalt Phosphide Catalyst for High-Efficiency Neutral-pH Water Splitting

Rui Wu et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2018)

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Article Chemistry, Physical

Sulfur-Doped Dicobalt Phosphide Outperforming Precious Metals as a Bifunctional Electrocatalyst for Alkaline Water Electrolysis

Mohsin Ali Raza Anjum et al.

CHEMISTRY OF MATERIALS (2018)

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Article Chemistry, Multidisciplinary

Regulating Water-Reduction Kinetics in Cobalt Phosphide for Enhancing HER Catalytic Activity in Alkaline Solution

Kun Xu et al.

ADVANCED MATERIALS (2017)

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Article Chemistry, Multidisciplinary

Mechanistic Insights on Ternary Ni2-xCoxP for Hydrogen Evolution and Their Hybrids with Graphene as Highly Efficient and Robust Catalysts for Overall Water Splitting

Jiayuan Li et al.

ADVANCED FUNCTIONAL MATERIALS (2016)

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Article Electrochemistry

Electrochemical impedance analysis of urea electro-oxidation mechanism on nickel catalyst in alkaline medium

Fen Guo et al.

ELECTROCHIMICA ACTA (2016)

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Article Crystallography

Manganese phosphide thin films and nanorods grown on gallium phosphide and on glass substrates

N. Nateghi et al.

JOURNAL OF CRYSTAL GROWTH (2016)

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Article Chemistry, Multidisciplinary

One-Step Synthesis of Self-Supported Nickel Phosphide Nanosheet Array Cathodes for Efficient Electrocatalytic Hydrogen Generation

Xiaoguang Wang et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2015)

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Article Chemistry, Physical

Deposition of β-Co(OH)2 Films by Electrochemical Reduction of Tris(ethylenediamine)cobalt(III) in Alkaline Solution

Jakub A. Koza et al.

CHEMISTRY OF MATERIALS (2013)

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Article Chemistry, Multidisciplinary

Electrochemical water splitting by layered and 3D cross-linked manganese oxides: correlating structural motifs and catalytic activity

Arno Bergmann et al.

ENERGY & ENVIRONMENTAL SCIENCE (2013)

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Article Electrochemistry

Understanding the electro-catalytic oxidation mechanism of urea on nickel electrodes in alkaline medium

Vedasri Vedharathinam et al.

ELECTROCHIMICA ACTA (2012)

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Article Chemistry, Multidisciplinary

Water-oxidation catalysis by manganese in a geochemical-like cycle

Rosalie K. Hocking et al.

NATURE CHEMISTRY (2011)

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Crystalline phosphides/amorphous oxides composite for energy-saving hydrogen production assisted by efficient urea oxidation reaction

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