期刊
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
卷 62, 期 2, 页码 -出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.202215094
关键词
Catalysis; Cross-Coupling; Mechanochemistry; Suzuki-Miyaura; Thermal Control
Several mechanochemically heated processes have been published, but precise control over mechanochemical catalysed coupling reactions has been difficult. A recent report demonstrates a programmable jar heater manifold that efficiently enables the Suzuki-Miyaura-type cross coupling reaction of aryl sulfamates and aryl boronic acid species. This methodology can be easily upscaled 200-fold using twin-screw extrusion methodologies.
Several mechanochemically heated processes have been published in recent years. However, precise control over the mechanochemical catalysed coupling reactions remained elusive. A recent report from Leitch, Browne and co-workers demonstrated how a programmable jar heater manifold delivers an efficient methodology for the Suzuki-Miyaura-type cross coupling reaction of aryl sulfamates and aryl boronic acid species. This methodology can be readily upscaled 200-fold using twin-screw extrusion methodologies.
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