期刊
CHEMISTRYSELECT
卷 7, 期 37, 页码 -出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/slct.202202968
关键词
amorfrutin A; amorfrutin B; total synthesis; Ru(II)-catalyzed olefination; 2; 4-dimethoxybenzoic acid
资金
- National Science Foundation of China [82060632]
- Scientific and Technological Talent Foundation of Guizhou Educational Committee [KY[2017]072]
- Guizhou High-level Innovative Talents Supporting Program [2016-4015]
- Guizhou Province Innovation Base of Common Major Chronic Disease Pathogenesis and Drug Development and Application [[2021]4029]
The convenient and facile syntheses of amorfrutin A and amorfrutin B have been successfully achieved in five steps starting from commercially available 2,4-dimethoxybenzoic acid, with overall yields of 32% and 22%, respectively. Key steps involved Ru(II)-catalyzed olefination and straightforward C-alkylation.
The convenient and facile syntheses of amorfrutin A and amorfrutin B have been realized in five steps starting from commercially available 2,4-dimethoxybenzoic acid with an overall yield of 32 % and 22 %, respectively. The key steps involved Ru(II)-catalyzed olefination and straightforward C-alkylation.
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