Helium-induced morphology evolution in tungsten under thermal treatment

Surface and near-surface morphology evolution of helium-irradiated tungsten due to thermal cycling up to the ITER-relevant temperature of 1350 K was studied using electron microscopy and positron annihilation spectroscopy techniques. Holes at the surface and bubbles in the near-surface of recrystallized polycrystalline tungsten samples were created by 75 eV helium plasma irradiation with the fluence of 3 x 10(23) He m(-2) at the surface temperature of 1073 K. Subsequent annealing experiments were combined with a detailed electron microscopy analysis to investigate the shape and density changes of holes and helium bubbles with respect to grain orientation. We show that the initially circular holes and round bubbles became faceted upon heating with 1 K s(-1) ramp up to 870 K. Annealing cycles up to 1350 K induced resulted in bubbles removal in the first 5 nm below the surface and surface smoothing. Electron energy loss spectroscopy measurements allowed estimation of helium gas density and pressure inside bubbles. Positron annihilation spectroscopy allowed to investigate the nature of defects and their evolution in the helium-irradiated tungsten with thermal cycling.

Automated summary

The evolution of surface and near-surface morphology of helium-irradiated tungsten during thermal cycling was studied using electron microscopy and positron annihilation spectroscopy. The results showed that the shape and density of holes and bubbles changed with thermal cycling, and the surface became smoother. Electron energy loss spectroscopy measurements and positron annihilation spectroscopy were used to investigate the properties and evolution of defects in the helium-irradiated tungsten.