4.7 Article

Hot isostatic pressing of Cu-15Ni-8Sn alloy with suppressed Sn macro-segregation and enhanced mechanical properties

出版社

ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2022.143866

关键词

Hot isostatic pressing (HIP); Cu-15Ni-8Sn alloy; Microstructural evolution; Mechanical properties; Sn segregation; Discontinuous precipitation (DP)

资金

  1. National Science and Technology Major Project [2017 -VI -0009-0080]
  2. National Natural Science Foundation of China [51905192, 51905193]
  3. China Postdoctoral Science Foundation [2021M701291, 2022TQ0110]
  4. Wuhan Science and Technology Project [2020010602012037]
  5. Hubei Province Provincial Teaching Research Project of Higher Education Institution [2020092]
  6. Teaching and Research Project at Huazhong University of Science and Technology [2019003]

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The use of hot isostatic pressing (HIP) technique in the fabrication of Cu-15Ni-8Sn alloy helps alleviate or eliminate macro-segregation and coarse grains issues, resulting in nearly fully dense samples with simultaneous strength-plasticity enhancement.
Sn macro-segregation and coarse grains easily occur in the conventional casting process of the Cu-15Ni-8Sn alloy with a high Sn content. Here, hot isostatic pressing (HIP), an advanced powder metallurgy technique, was introduced to explore feasibility in alleviating or eliminating such defects. The gas-atomized powder with high homogeneity of composition was used, which was solidified rapidly. The microstructural evolution, mechanical properties, deformation mechanisms and strengthening mechanisms were deeply and systematically revealed and discussed. Nearly fully dense samples were fabricated by HIP with no Sn macro-segregation, and simulta-neous strength-plasticity enhancement was obtained. The content of harmful discontinuous precipitation col-onies was controlled to only-3.11 vol%. This was attributed to the fine grain size of the powder and the preferential complete recrystallization process during the HIP. That is, the gamma nucleation sites were occupied by numerous grain boundaries provided by fine grains, and the driving force of gamma growth was consumed by recrystallization. Furthermore, enhanced mechanical properties were related to the Sn macro-segregation sup-pression, grain refinement (-11.0 mu m), dislocation density continuous increase, and dispersion distribution of gamma precipitates, etc. These encouraging findings validate the advantages and potential of HIP in the fabrication of Cu-15Ni-8Sn alloy with enhanced mechanical properties for structural applications.

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