4.7 Article

Synthesis of Heterobenzyl Sulfoxides Enabled by Palladium- Catalyzed Allylic Alkylation of Sulfenate Anions with Allenamides

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JOURNAL OF ORGANIC CHEMISTRY
卷 -, 期 -, 页码 -

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AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.2c01998

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资金

  1. National Natural Science Foundation of China
  2. Natural Science Foundation of Jiangsu Province
  3. Lvyang Jinfeng Talents Attracting Plan
  4. [22101249]
  5. [BK20200918]

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A highly efficient palladium-catalyzed allenamide allylic alkylation of sulfenate anions under mild conditions is demonstrated, providing a practical protocol to access various sulfoxide-containing heterocyclic compounds. The transformation features a broad substrate scope, good functional group tolerance, easy scalability, and convenient synthetic transformation.
A highly efficient palladium-catalyzed allenamide allylic alkylation of sulfenate anions under mild conditions is demonstrated. The present methodology provides a practical protocol to access various sulfoxide-containing heterocyclic compounds. The salient features of this transformation include a broad substrate scope, good functional group tolerance, easy to scale-up, and ready synthetic transformation.

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