☆ 4.7 Review

Recent developments in the field of dehydration of bio-renewable glycerol to acrolein over molecular sieve catalysts

JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY (2023)

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Ni-based catalysts supported on acid/alkali-activated coal fly ash residue for improved glycerol steam reforming

Kang Gao et al.

Summary: The physicochemical properties of low-efficiency coal fly ash were significantly improved through simple acid/alkali treatments, enhancing the catalytic activity for glycerol steam reforming. Alkali-LPD proved more effective than acid-LPD in improving the surface area and elemental distribution of the fly ash.

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Kinetic study of glycerol steam reforming catalyzed by a Ni-promoted metallurgical residue

Alex Desgagnes et al.

Summary: The study investigated the kinetics of glycerol steam reforming reaction catalyzed by a nickel-promoted metallurgical residue in a fixed-bed reactor at atmospheric pressure. The most accurate and thermodynamically consistent mechanism involved the dissociative adsorption of glycerol, which led to the breaking of C-C bonds and dehydrogenation of glycerol as the rate-determining step. The activation energy was found to be 66.1 kJ.mol-1 with a partial order with respect to glycerol of 0.63, as validated by a macroscopic analysis of glycerol to gas consumption rates.

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Article Chemistry, Applied

Conversion of glycerol over vanadium supported beta zeolite: Role of acidity and alkali cations

Auguste Fernandes et al.

Summary: Vanadium supported beta zeolite catalysts modified with Cs and K can convert glycerol into allyl alcohol in gas phase. The presence of vanadium oxide species promotes allyl alcohol formation, while modification with Cs or K changes vanadium species and highlights the importance of acidity in the process. The formation of allyl alcohol is favored by a low density of acid sites, at the expense of acrolein formation, and the data suggest a closely related mechanistic path for both compounds.

MICROPOROUS AND MESOPOROUS MATERIALS (2022)

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Review Green & Sustainable Science & Technology

A review on recent developments and progress in sustainable acrolein production through catalytic dehydration of bio-renewable glycerol

Anas Abdullah et al.

Summary: The catalytic dehydration of glycerol to acrolein is a promising research topic with commercial prospects. Recent studies have focused on reducing catalyst deactivation, improving catalyst stability, and optimizing reaction parameters. Promising results have been achieved through altering catalyst structure, introducing new techniques and methods.

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Design of a naphthalimide-based probe for acrolein detection in foods and cells

Kaiyu Jiang et al.

Summary: In this study, a novel fluorescent probe Pr-ACR was designed and synthesized for highly sensitive and specific detection of acrolein. It was found that the probe could quantitatively detect acrolein in foods and visualize acrolein in cells.

JOURNAL OF HAZARDOUS MATERIALS (2022)

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Article Chemistry, Applied

Mesoporous silica supported phosphotungstic acid catalyst for glycerol dehydration to acrolein

Zhiheng Wang et al.

Summary: In this study, tungsten-based heteropolyacids supported on non-ordered mesoporous silica were investigated as catalysts for glycerol dehydration to acrolein. Characterization and analysis revealed the surface structure of HPA, the acidic properties, and the correlation between acidic properties and dehydration activity. The results showed that acrolein yield increased with H3PW12O40 loading until 30 wt%, discussing the active role of Bronsted acid and the cooperative role of Bronsted/Lewis acid sites for glycerol dehydration to acrolein.

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A review on one-pot synthesis of acrylic acid from glycerol on bi-functional catalysts

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Summary: Oxydehydration of glycerol to acrylic acid is a two-step reaction involving dehydration and oxidation, requiring careful catalyst selection and reaction condition control to achieve high yield. The review focuses on recent works and critical analysis of different catalysts, highlighting the importance of specific acid sites and redox strength of active components.

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Insight into the Mechanism of Glycerol Dehydration and Subsequent Pyridine Synthesis

Ding Jiang et al.

Summary: In this study, glycerol was used to synthesize pyridine, and it was found that neutral glycerol could be directly converted into pyridine in an ammonia atmosphere. The research confirmed the conversion mechanism with experimental data and theoretical modeling. Additionally, the ZSM-5 catalyst played a role in shape-selectivity and altering the reaction pathway for glycerol conversion to pyridine.

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Catalytic Deactivation of HY Zeolites in the Dehydration of Glycerol to Acrolein

Israel Pala-Rosas et al.

Summary: The study found that increasing the SiO2/Al2O3 molar ratio of HY zeolites decreases the total amount of acid sites per unit area, leading to a reduced initial glycerol conversion; however, the initial acrolein selectivity increases with the higher Brønsted/Lewis acid sites ratio. The catalyst lifetime depends on pore structure, with larger surface areas improving deactivation rate constants.

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Bio-removal of phenol by the immobilized laccase on the fabricated parent and hierarchical NaY and ZSM-5 zeolites

Atefeh Ameri et al.

Summary: This study synthesized NaY and ZSM-5 zeolites and their hierarchical forms, which exhibited increased pore size and mesoporous pore volume. Immobilized laccases showed enhanced thermal and pH stability, with over 50% activity retained after storage. The hierarchical forms of immobilized laccases demonstrated higher efficiency in phenol removal and exhibited good reusability after multiple cycles.

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Comparison of carbon molecular sieve and zeolite 5A for CO2 sequestration from CH4/CO2 mixture gas using vacuum pressure swing adsorption

Daeho Ko

Summary: The study compared the performance of carbon molecular sieves and zeolite 5A in a four-bed vacuum pressure swing adsorption process, finding that each has its own advantages under different operating conditions. Carbon molecular sieves perform better in purity enhancement under high vacuum pressure, while zeolite 5A has better power efficiency under low-pressure operating conditions.

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Summary: The study revealed systematic differences in crystallinity, morphology, and acidity between nanosized and microsized H-ZSM-5 zeolites. Only a portion of framework aluminium atoms in nanosized materials contribute to forming Br?nsted acidic bridging OH groups, while the rest lead to the formation of silanol groups with weakly enhanced Br?nsted acidity.

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Progress of the Catalytic Deactivation of H-ZSM-5 Zeolite in Glycerol Dehydration

Gabriel L. Catuzo et al.

Summary: This study investigates the detailed aging of coke in spent H-ZSM-5 zeolites after their use in the gas-phase glycerol dehydration to produce acrolein. The carbonaceous deposits formed rapidly in the pores hampering the accessibility to active sites and the zeolite's catalytic action. The types of coke formed during the reaction and their impact on the zeolite's structure and accessibility to acid sites were also examined.

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Hydrogen production via methane decomposition over nickel supported on synthesized ZSM-5/MCM-41 zeolite composite material

Lilia Alalga et al.

Summary: The catalytic decomposition of methane for COx-free hydrogen production was successfully achieved using 20 wt% Ni supported on H-ZSM-5/MCM-41 composite material. The composite material exhibited higher catalytic activity and stability, possibly due to improved access to active Ni metal atoms and their dispersion. This study provides valuable insights into the development of efficient catalysts for hydrogen production.

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Green and facile synthesis of glycerol carbonate from bio-glycerol assisted by lithium titanate: A robust and selective heterogeneous catalyst

Siddhi Jaiswal et al.

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JOURNAL OF THE TAIWAN INSTITUTE OF CHEMICAL ENGINEERS (2021)

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Direct surface modification of mesoporous silica nanoparticles by DBD plasma as a green approach to prepare dual-responsive drug delivery system

Sahar Porrang et al.

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In situ growth of hierarchical SAPO-34 loaded with Pt for evolution hydrogen production from hydrolysis of AB

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Byung Jin Lee et al.

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MICROPOROUS AND MESOPOROUS MATERIALS (2021)

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Tuning of Selectivity for Sustainable Production of Acrolein from Glycerol

Artem S. Belousov

Summary: The article discusses the catalytic dehydration of glycerol into acrolein, highlighting key approaches for enhancing selectivity by altering physicochemical properties of catalysts and optimizing reaction conditions. Metal-organic frameworks are proposed as novel catalysts to address challenges in glycerol dehydration.

CHEMISTRYSELECT (2021)

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Lithium loaded coal fly ash as sustainable and effective catalyst for the synthesis of glycerol carbonate from glycerol

Shivali Arora et al.

Summary: In this study, coal fly ash was utilized as a catalytic support for lithium ions by impregnation, with the resulting catalyst's basic properties and catalytic activity towards glycerol conversion being experimentally determined. The maximum catalytic activity was achieved with 2 wt% lithium loaded CFA, calcined at 500 degrees C, leading to a maximum yield of glycerol carbonate. The proposed work has the potential to potentially boost the economy of the biodiesel industry.

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Methane combustion over palladium catalyst within the confined space of MFI zeolite

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Renewable hydrogen from glycerol steam reforming using Co-Ni-MgO based SBA-15 nanocatalysts

S. Al-Salihi et al.

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Continuous catalytic process for the selective dehydration of glycerol over Cu-based mixed oxide

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Oxidative dehydrogenation of propane using layered borosilicate zeolite as the active and selective catalyst

Bin Qiu et al.

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Controlling the selectivity and deactivation of H-ZSM-5 by tuning b-axis channel length for glycerol dehydration to acrolein

Babar Ali et al.

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Gas-phase dehydration of glycerol to acrolein over different metal phosphate catalysts

Tianlin Ma et al.

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Cooperation of hierarchical pores with strong Bronsted acid sites on SAPO-34 catalysts for the glycerol dehydration to acrolein

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Gas-phase dehydration of glycerol to acrolein catalyzed by hybrid acid sites derived from transition metal hydrogen phosphate and meso-HZSM-5

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Glycerol dehydration over micro- and mesoporous ZSM-5 synthesized from a one-step method

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Nanosheet MFI Zeolites for Gas Phase Glycerol Dehydration to Acrolein

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Microwave-assisted catalytic dehydration of glycerol for sustainable production of acrolein over a microwave absorbing catalyst

Qinglong Xie et al.

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Interface synergy between IrOx and H-ZSM-5 in selective C-O hydrogenolysis of glycerol toward 1,3-propanediol

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Gas phase glycerol dehydration over H-ZSM-5 zeolite modified by alkaline treatment with Na2CO3

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Gas phase dehydration of glycerol to acrolein over CS2.5H0.5PW12O40/Zr-MCM-41 catalysts prepared by supercritical impregnation

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Facile Synthesis of a Novel Hierarchical ZSM-5 Zeolite: A Stable Acid Catalyst for Dehydrating Glycerol to Acrolein

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Sulfonic functionalized SBA-15 catalysts in the gas phase glycerol dehydration. Thermal stability and catalyst deactivation

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Glycerol dehydration catalyzed by MWW zeolites and the changes in the catalyst deactivation caused by porosity modification

Mariana V. Rodrigues et al.

APPLIED CATALYSIS A-GENERAL (2015)

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Supported H4SiW12O40/Al2O3 solid acid catalysts for dehydration of glycerol to acrolein: Evolution of catalyst structure and performance with calcination temperature

Licheng Liu et al.

APPLIED CATALYSIS A-GENERAL (2015)

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Kinetic Modeling, Thermodynamic, and Mass-Transfer Studies of Gas-Phase Glycerol Dehydration to Acrolein over Supported Silicotungstic Acid Catalyst

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INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH (2015)

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Vapor Phase Dehydration of Glycerol to Acrolein Over SBA-15 Supported Vanadium Substituted Phosphomolybdic Acid Catalyst

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JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY (2015)

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Dehydration of glycerol to acrolein using H-ZSM5 zeolite modified by alkali treatment with NaOH

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MICROPOROUS AND MESOPOROUS MATERIALS (2015)

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Dehydration of Glycerol to Acrolein over Hierarchical ZSM-5 Zeolites: Effects of Mesoporosity and Acidity

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ACS CATALYSIS (2015)

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Gas-phase dehydration of glycerol over thermallystable SAPO-40 catalyst

J. P. Lourenco et al.

RSC ADVANCES (2015)

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Article Chemistry, Physical

Gas phase dehydration of glycerol over, lanthanum-modified beta-zeolite

B. O. Dalla Costa et al.

APPLIED CATALYSIS A-GENERAL (2014)

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Article Chemistry, Applied

Catalytic dehydration of glycerol to acrolein over HPW supported on Cs+ modified SBA-15

Rong Liu et al.

CATALYSIS TODAY (2014)

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Article Engineering, Chemical

In situ synthesized nano-copper over ZSM-5 for the catalytic dehydration of glycerol under mild conditions

Chuan-Jun Yue et al.

JOURNAL OF THE TAIWAN INSTITUTE OF CHEMICAL ENGINEERS (2014)

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Review Green & Sustainable Science & Technology

Glycerol for renewable acrolein production by catalytic dehydration

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RENEWABLE & SUSTAINABLE ENERGY REVIEWS (2014)

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Article Chemistry, Physical

Cooperativity of Bronsted and Lewis Acid Sites on Zeolite for Glycerol Dehydration

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ACS CATALYSIS (2014)

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Metal oxides nanoparticles from complexes on SBA-15 for glycerol conversion

Francisco F. de Sousa et al.

CHEMICAL ENGINEERING JOURNAL (2013)

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Article Chemistry, Physical

Performance of ZrO2-supported Nb- and W-oxide in the gas-phase dehydration of glycerol to acrolein

Mariano Massa et al.

JOURNAL OF CATALYSIS (2013)

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Article Chemistry, Physical

A comparative study of glycerol dehydration catalyzed by micro/mesoporous MFI zeolites

Luiz Gustavo Possato et al.

JOURNAL OF CATALYSIS (2013)

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Article Chemistry, Applied

Efficiency of zeolite MCM-22 with different SiO2/Al2O3 molar ratios in gas phase glycerol dehydration to acrolein

Camila S. Carrico et al.

MICROPOROUS AND MESOPOROUS MATERIALS (2013)

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Article Chemistry, Physical

Study on the influence of channel structure properties in the dehydration of glycerol to acrolein over H-zeolite catalysts

Yunlei Gu et al.

APPLIED CATALYSIS A-GENERAL (2012)

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Article Chemistry, Physical

Zirconium doped mesoporous silica catalysts for dehydration of glycerol to high added-value products

C. Garcia-Sancho et al.

APPLIED CATALYSIS A-GENERAL (2012)

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Article Chemistry, Physical

Sulfonic-functionalized SBA-15 as an active catalyst for the gas-phase dehydration of Glycerol

Joao P. Lourenco et al.

CATALYSIS COMMUNICATIONS (2012)

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A comparative study for gas-phase dehydration of glycerol over H-zeolites

Yong Tae Kim et al.

APPLIED CATALYSIS A-GENERAL (2011)

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Degradation of glycerol using hydrothermal process

Lailatul Qadariyah et al.

BIORESOURCE TECHNOLOGY (2011)

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Catalytic conversion of glycerol to acrolein over modified molecular sieves: Activity and deactivation studies

Aldenor S. de Oliveira et al.

CHEMICAL ENGINEERING JOURNAL (2011)

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A Revisited Picture of the Mechanism of Glycerol Dehydration

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JOURNAL OF PHYSICAL CHEMISTRY A (2011)

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Catalytic conversion of glycerol to value added liquid products

Kapil Pathak et al.

APPLIED CATALYSIS A-GENERAL (2010)

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Article Chemistry, Physical

Small-sized HZSM-5 zeolite as highly active catalyst for gas phase dehydration of glycerol to acrolein

Chun-Jiang Jia et al.

JOURNAL OF CATALYSIS (2010)

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Gas-phase dehydration of glycerol over ZSM-5 catalysts

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MICROPOROUS AND MESOPOROUS MATERIALS (2010)

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Acidic catalysts for the dehydration of glycerol: Activity and deactivation

Wladimir Suprun et al.

JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL (2009)

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Biomass to chemicals: Catalytic conversion of glycerol/water mixtures into acrolein, reaction network

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Acrolein synthesis from glycerol in hot-compressed water

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BIORESOURCE TECHNOLOGY (2007)

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Sustainable production of acrolein: investigation of solid acid-base catalysts for gas-phase dehydration of glycerol

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GREEN CHEMISTRY (2007)

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Catalytic dehydration of glycerol in sub- and supercritical water: a new chemical process for acrolein production

L Ott et al.

GREEN CHEMISTRY (2006)

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Hierarchical zeolites: A proven strategy to combine shape selectivity with efficient mass transport

M Hartmann

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2004)

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