期刊
CERAMICS INTERNATIONAL
卷 48, 期 19, 页码 28299-28307出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2022.06.137
关键词
Hydroxyapatite; Ultrasonication; Nanoparticles; Biowaste; Hyperthermia
资金
- King Khalid University, Abha, Saudi Arabia [G.P.2/82/43]
This study successfully conducted one-pot ultrasonic-assisted synthesis of magnetic HAp nanoparticles, developed a HAp/Fe3O4 nanocomposite with good magnetic induction heating ability by incorporating Fe2+/Fe3+ ions, and showed potential application value.
The studies on hydroxyapatite (HAp) nanoparticles have prompted prospects for superior biomaterials in or-thopedics and dentistry. In this work, one-pot ultrasonic-assisted synthesis of magnetic HAp nanoparticles was carried out using a mussel shell calcium source by incorporating Fe2+/Fe3+ ions during Ca-citrate complex formation. Characterization of prepared specimens revealed that Fe2+/Fe3+ ions integration at low concentrations (0.01:0.02 ratio) does not affect the phase purity of HAp nanoparticles while at high concentrations (0.1:0.2 ratio) produced HAp/Fe3O4 nanocomposite. The developed HAp/Fe3O4 nanocomposite was composed of spherical Fe3O4 nanoparticles (10 nm size) and rod-like HAp nanoparticles (5-10 nm width and 20-30 nm length), and it revealed soft ferromagnetic properties with coercivity (Hc) and saturation magnetization (Ms) values of 750 G and 7.05 emu/g, respectively. Furthermore, the developed HAp/Fe3O4 nanocomposite exhibited good bone-forming ability in SBF and accomplished hyperthermia temperature within 8 min at 400 A applied current. Hence, it can be a potential bone repair material with magnetic induction heating ability. Also, this study utilized mussel shell calcium precursor which is a cost-effective and ecologically friendly method.
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