期刊
CERAMICS INTERNATIONAL
卷 48, 期 19, 页码 28072-28081出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2022.06.112
关键词
Environmental barrier coatings; SiC whisker; Spray drying; Vacuum sintering
资金
- National Science and Technology Major Project of the Ministry of Science and Technology of China [2017-VI-0020-0093]
- Natural Science Project of Heilongjiang Provincial Department of Education [145109119]
Yb2Si2O7 powders doped with SiC whisker were prepared as feed stocks for environmental barrier coatings through ball milling, spray drying, and vacuum sintering. The particle size of the powder can be optimized by adjusting the spray drying parameters. Vacuum sintering improves the density and flowability of the powders, while the SiC whisker maintains its original morphology.
In order to prolong the lifetime of environmental barrier coatings (EBCs) produced by thermal spraying, Yb2Si2O7 powders doped with SiC whisker(SiCw/Yb2Si2O7) as feed stocks was prepared by ball milling, spray drying and vacuum sintering. The morphology, phase composition, particle size, flowability and densification of the powder were analyzed by TG-DSC, XRD, SEM and other methods. The SiC whisker was wrapped into the nanometer agglomerated powder by spray drying. The particle size varied by different spray drying parameters. Powders used for atmospheric plasma spraying were prepared by spray drying, optimal particle size can be obtained under 250 degrees C inlet temperature, 0.05 MPa atomization pressure, and a peristaltic pump rate of 60 r/ min. With the increase of vacuum calcination temperature, the density and flowability of powders are improved, and the composition of the powder changed from Yb2O3 to Yb2SiO5 and finally to Yb2Si2O7. The optimal compactness and flowability of the powders were obtained at the sintering temperature of 1300 degrees C with minimal surface porosity. SiC whisker was not oxidized during the vacuum sintering and still maintained the original whisker morphology. The densification process of recombinant particles and its mechanism were analyzed in terms of surface morphology and cross section.
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