☆ 4.6 Review

Recent advances in oxidative dehydrogenation of propane to propylene on boron-based catalysts

CATALYSIS REVIEWS-SCIENCE AND ENGINEERING (2022)

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Water-Tolerant Boron-Substituted MCM-41 for Oxidative Dehydrogenation of Propane

Qingying Liu et al.

Summary: Mesoporous B-MCM-41 catalysts with varying boron content (B/Si = 0.015-0.147) were prepared using a simple hydrothermal synthesis method. The catalyst with B/Si = 0.048 exhibited favorable activity, stability, and water tolerance in the oxidative dehydrogenation of propane reaction. The active sites for ODHP were identified as the tri-coordinated B-OH species incorporated into the mesoporous silica framework.

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Article Chemistry, Physical

Borosilicate zeolite enriched in defect boron sites boosting the low-temperature oxidative dehydrogenation of propane

Bin Qiu et al.

Summary: In this study, an incompletely crystallized borosilicate zeolite catalyst exhibited extraordinary performance in the oxidative dehydrogenation of propane. The boron species were found to be anchored to the zeolite matrix in the form of open coordination and formed hydrogen bonds with defective boron species, preventing excessive leaching of boron. The active center for catalyzing the reaction was identified as the B-OH groups in aggregated BOx species that formed hydrogen bonds with adjacent Si-OH groups.

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Engineering O-O Species in Boron Nitrous Nanotubes Increases Olefins for Propane Oxidative Dehydrogenation

Panpan Li et al.

Summary: In this study, boron-oxygen-nitrogen nanotubes (BONNTs) enriched with O-O species were developed as a highly active, selective, and stable catalyst for oxidative propane dehydrogenation (OPDH).

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Article Chemistry, Multidisciplinary

Multiple Promotional Effects of Vanadium Oxide on Boron Nitride for Oxidative Dehydrogenation of Propane

Xiao Jiang et al.

Summary: We report a catalyst with vanadium oxide dispersed onto hexagonal boron nitride (h-BN), which catalyzes the oxidative dehydrogenation of propane (ODHP) via the Eley-Rideal mechanism and the Mars-van Krevelen mechanism. The results show that loading 0.5wt% V significantly improves the yield of light alkene. Adding an appropriate concentration of nitric oxide further enhances the catalytic performance. This provides a potential strategy for developing efficient h-BN-based catalysts for ODHP by coupling gas-phase and surface reactions.

JACS AU (2022)

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Nanoscale Hybrid Amorphous/Graphitic Carbon as Key Towards Next-Generation Carbon-Based Oxidative Dehydrogenation Catalysts

Felix Herold et al.

Summary: A new synthesis strategy utilizing non-nano carbon materials as dehydrogenation catalysts has been developed, allowing for control over macroscopic shape, texture, and crystallinity. By fine-tuning the synthesis, high selectivity active carbon catalysts similar to carbon nanotubes can be obtained, with significantly higher space-time yields in test reactions. This new class of carbon materials is technically scalable, reproducible, and exhibits spherical particles for easy handling.

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Review Chemistry, Physical

Catalyst design and tuning for oxidative dehydrogenation of propane - A review

Yahya Gambo et al.

Summary: This study comprehensively reviews recent advances in key aspects related to ODHP catalysts, discussing active site nature, isolation, accessibility, and other properties, as well as exploring accelerated discovery of novel catalysts and the application of machine learning frameworks.

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Nonmetal oxygen vacancies confined under boron nitride for enhanced oxidative dehydrogenation of propane to propene

Qiuwen Liu et al.

Summary: In this study, oxygen vacancies-rich BPO4 hollow spheres covered with few-layer hexagonal boron nitride (BN) were prepared, showing better catalytic activity and selectivity in the oxidative dehydrogenation of propane to propene compared to commercial BN due to the synergistic effect between oxygen vacancies-rich BPO4 and h-BN. Oxygen vacancies enhance propane adsorption while the confined space at the interface weakens propene adsorption, facilitating active site recycling. The confined space and oxygen vacancies also lead to a transformation in the reaction kinetic model.

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Modulating the crystallinity of boron nitride for propane oxidative dehydrogenation

Tian-Chang Wang et al.

Summary: In this study, the catalytic performance of h-BN in propane oxidative dehydrogenation was improved by modulating the catalyst crystallinity, leading to a significant increase in propane conversion rate. Additionally, the high crystallinity of BN was proven to be beneficial for O-2 binding, reducing the energy barrier for O-2 activation.

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It's a Gas: Oxidative Dehydrogenation of Propane over Boron Nitride Catalysts

Peter Kraus et al.

Summary: The study suggests that boron nitride catalysts exhibit high selectivity in the oxidative dehydrogenation of propane, which can be modeled reasonably well by a gas-phase conversion mechanism. Water cofeed leads to increased conversion of propane, while dilution of the catalytic bed and variations in the C3H8/O-2 ratio also affect the selectivities of minor species in gas-phase reactions.

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Review Chemistry, Physical

Oxidative Dehydrogenation of Propane to Propylene with Soft Oxidants via Heterogeneous Catalysis

Xiao Jiang et al.

Summary: Oxidative dehydrogenation of propane to propylene can be achieved using conventional oxygen-assisted dehydrogenation or soft oxidants. Soft oxidants play important roles in inhibiting overoxidation and improving propylene selectivity. Significant efforts have been focused on developing different catalysts with recent emphasis on halogens and hydrogen halides for ODHP processes.

ACS CATALYSIS (2021)

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Fabrication of h-BN/SiO2 Nanofibers Showing High Olefins Productivity in Oxidative Dehydrogenation of Propane

Ding Ding et al.

Summary: This study focused on the preparation of one-dimensional nanofiber catalysts consisting of hexagonal boron nitride/silica oxide (h-BN/SiO2) via electrospinning method, showing high conversion rate and selectivity towards propylene in oxidative dehydrogenation of propane (ODHP). The findings suggest a new strategy for preparing efficient boron-based catalysts for ODHP process.

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Isolated boron in zeolite for oxidative dehydrogenation of propane

Hang Zhou et al.

Summary: Isolated boron in a zeolite framework without B-O-B oligomers exhibits high activity and selectivity for oxidative dehydrogenation of propane (ODHP). The boron-silicon bonding structure hinders boron leaching in a humid atmosphere, enhancing catalyst durability. The -B[OH center dot center dot center dot O(H)-Si](2) structure in borosilicate zeolite serves as the active center for activating oxygen and carbon-hydrogen bonds to catalyze ODHP.

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Plasma Tuning Local Environment of Hexagonal Boron Nitride for Oxidative Dehydrogenation of Propane

Zhankai Liu et al.

Summary: The study found that N2-treated hexagonal boron nitride showed remarkable activity with good selectivity towards propane, while O2 treatment led to sintering effect of BOx species which suppressed the catalytic performance.

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Understanding the origin of selective oxidative dehydrogenation of propane on boron-based catalysts

Jinshu Tian et al.

Summary: This study demonstrates that oxidized boron species in boron-based catalysts serve as active sites for highly selective olefin formation. Furthermore, the high selectivity of olefins in ODHP on such catalysts is attributed to the suppressed adsorption of olefins on >B-O-O-B< sites.

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Highly Selective Carbon-Supported Boron for Oxidative Dehydrogenation of Propane

Lesli O. Mark et al.

Summary: Bulk boron materials, such as hexagonal boron nitride (h-BN), are highly selective catalysts for the oxidative dehydrogenation of propane. Previous attempts to improve productivity by immobilizing boron on silica led to less selective catalysts. Acid-treated, activated carbon-supported boron (B/OAC) prepared via incipient wetness impregnation exhibits equal propylene selectivity and improved productivity compared to h-BN, with oxidized/hydrolyzed boron clustered on the support surface.

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Controlled Grafting Synthesis of Silica-Supported Boron for Oxidative Dehydrogenation Catalysis

Melissa C. Cendejas et al.

Summary: The study focused on the controlled grafting synthesis of pinacolborane on amorphous silica, revealing that the silica pretreatment dehydration temperature can control the formation of hydrogen bonds. Thermal treatment under vacuum showed that boron on the silica surface is highly mobile at elevated temperatures, and the catalysts exhibited expected activity. However, the kinetic behavior of these supported catalysts deviates from that of bulk boron materials, prompting further research into reaction kinetics.

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Summary: This study investigates the mechanism of boron-based catalysts in inhibiting alkane deep-oxidation through density functional theory calculations and electronic and geometric structure analysis. It reveals that surface boron sites can eliminate alkoxyl groups nearby, leading to exceptional inhibition of alkane deep-oxidation. Furthermore, the oxophilicity of boron is found to be crucial in determining the low deep-oxidation of alkanes.

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Effect of secondary additives on the properties of vanadium-aluminum mixed oxide tableted catalysts used in the oxidation of propane

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Huan Yan et al.

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Interplay of On- and Off-Surface Processes in the B2O3-Catalyzed Oxidative Dehydrogenation of Propane: A DFT Study

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Summary: Metal-free boron-based catalytic systems show promising potential in the oxidative dehydrogenation of light alkanes to olefins. Understanding the interplay between on-surface and off-surface channels is crucial for maintaining high selectivity and conversion rates in the reaction, as demonstrated in this study using density functional theory.

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