期刊
JOURNAL OF ENERGETIC MATERIALS
卷 35, 期 3, 页码 314-320出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/07370652.2016.1190795
关键词
2,4,4,6,6,8,8,(9).0(3),10,10,(11) dodecane; 12-hexaazatetracyclo 5.5.0.0(5); 12-hexabenzyl-2; CL-20 explosive precursor; CuFe2O4 MNPs; magnetic nanoparticles of copper ferrite; reusable catalyst
类别
资金
- University of Sistan and Baluchestan
Magnetic nanoparticles of copper ferrite (CuFe2O4 MNPs) have been simply prepared and applied as an efficient recyclable and reusable catalyst for the green synthesis of 2,4,6,8,10,12-hexabenzyl-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0(5,9).0(3,11)]dodecane (HBIW). The structure of the synthesized pure HBIW (recrystallization from ethanol) was confirmed by using various spectral techniques like infrared (IR), H-1-NMR, C-13-NMR and some of its physical properties. The prepared catalyst was characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and Fourier transform infrared (FTIR). In addition, CuFe2O4 MNPs could be reused up to seven runs without any significant loss of activity. Finally, the remarkable advantages of this method are the simple experimental procedure, shorter reaction times, simple workup, and green aspects by avoiding toxic catalysts and high yield of product.
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