Synthesis and crystal structure of 1-((3R,10S,13R,17S)-10,13-dimethyl-3-(phenylamino)hexadecahydro-1H-cyclopenta[α] phenanthren-17-yl)ethan-1-one, C27H39NO

C27H39NO, orthorhombic, P2(1)2(1)2(1) (no. 19), a = 10.5248(7) angstrom, b = 12.6248(7) angstrom, c = 16.8913(9) angstrom, V = 2244.4(2) angstrom(3), Z = 4, R-gt (F) = 0.0435, wR(ref) (F (2)) = 0.1033, T = 173(2) K.

Automated summary

C27H39NO compound was found to have orthorhombic crystal structure with space group P2(1)2(1)2(1) (no. 19). The unit cell parameters were determined to be a = 10.5248(7) angstrom, b = 12.6248(7) angstrom, c = 16.8913(9) angstrom, and the volume V = 2244.4(2) angstrom(3). The crystal structure contains 4 molecules, and the refined R-factor R-gt (F) is 0.0435 with weighted R-factor wR(ref) (F (2)) of 0.1033 at a temperature of 173(2) K.