期刊
TETRAHEDRON LETTERS
卷 104, 期 -, 页码 -出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2022.154041
关键词
Disulfenylation; Hypervalent iodine; Thiophene; Thiyl radical
资金
- National Natural Science Foundation of China [U2001222, 21975055, 21975053]
- Guangdong Basic and Applied Basic Research Foundation [2019B1515120023]
- Science and Technology Planning Project of Guangdong Province [2021A0505030069]
A hypervalent iodine-induced disulfenylation of thiophene derivatives with thiophenols via a thiyl radical reaction pathway has been achieved. This transformation provides direct synthetic access to 2,3-disulfenylated thiophene derivatives in 34-78% yields with good functional group compatibility under mild reaction conditions.
A hypervalent iodine-induced disulfenylation of thiophene derivatives with thiophenols via a thiyl radical reaction pathway has been achieved. This transformation provides direct synthetic access to 2,3-disulfenylated thiophene derivatives in 34-78% yields with good functional group compatibility under mild reaction conditions. (C) 2022 Elsevier Ltd. All rights reserved.
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