期刊
ORGANIC LETTERS
卷 24, 期 23, 页码 4109-4113出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.2c01099
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资金
- RWTH Aachen University
The first mechanochemical synthesis of sulfonimidamides is reported in this study. This one-pot, two-step method does not require a solvent or inert conditions. Sulfinamides are rapidly converted to sulfonimidoyl chlorides through oxidative chlorination with N-chlorosuccinimide (NCS) in a mixer mill, followed by substitution with amines to provide a wide range of diversely substituted sulfonimidamides.
Here, we report the first mechanochemical synthesis of sulfonimidamides. The one-pot, two-step method requires neither a solvent nor inert conditions. In a mixer mill, sulfinamides are rapidly converted to sulfonimidoyl chlorides by oxidative chlorination with N-chlorosuccinimide (NCS). Subsequent substitutions with amines provides a wide range of diversely substituted sulfonimidamides.
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