期刊
LANGMUIR
卷 38, 期 30, 页码 9285-9293出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.langmuir.2c01042
关键词
-
资金
- Vietnam National Foundation for Science and Technology Development (NAFOSTED) under g r a n [106.02.2018.315]
- Vietnam National Foundation for Science and Technology Development (NAFOSTED) [106.02.2018.315]
This study developed a green method of ultrasound-assisted extraction coupled with gas bubble flotation for extracting fi-amyrin from Dischidia major. The solvent system used was water:ethanol (9:1) and cationic surfactants were employed to improve the adsorption of fi-amyrin onto the air/liquid interface during flotation. High-performance liquid chromatography with spectrophotometric detection was applied to quantify the fi-amyrin content in D. major and its extracts. The foam layer collected from flotation showed high selectivity toward fi-amyrin, and the product content increased significantly after removing surfactants from the solution.
Ultrasound-assisted extraction coupled with gas bubble flotation was developed as a green method for extracting fi-amyrin fromDischidia major. The solvent system was water:ethanol (9:1). To improve the adsorption of fi-amyrin onto the air/liquid interface during flotation, surfactants were employed; however, the positive effect was only observed with cationic surfactants. High-performance liquid chromatography with spectrophotometric detection (HPLC-PDA) was, for the first time, applied to quantify the fi-amyrin content in D. major and its extracts. With the assistance of surfactants, the foam layer collected from flotation showed high selectivity toward fi-amyrin. The product content was notably increased after surfactants had been removed from the solution.
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