4.4 Article

The effects of experimental etchant with calcium phosphate ion clusters on the nanoleakage at dentin-resin hybrid layer

期刊

JOURNAL OF ADHESION SCIENCE AND TECHNOLOGY
卷 37, 期 11, 页码 1756-1769

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TAYLOR & FRANCIS LTD
DOI: 10.1080/01694243.2022.2093567

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Dentin; calcium phosphates; resin; adhesive

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This study investigated the potential of a calcium phosphate ion cluster-incorporating phosphoric acid solution to enhance remineralization of the hybrid layer and prevent nanoleakage at the dentin-resin interface, resulting in improved long-term bonding strength.
This study aimed to investigate the possibility that a calcium phosphate ion cluster (CPIC)-incorporating phosphoric acid (PA) solution promotes the remineralization of the hybrid layer and prevents nanoleakage from the dentin-resin interface, thereby minimizing dentin-resin bond failure during long-term bonding periods. The specimens were prepared using human molars and treated with three types of etching solutions (35% PA, and CPIC-incorporated PA solutions at 1:1 and 1:2 ratios). The microtensile bond strength (mu TBS) of half of the specimens was measured after 24 h, and measured after thermocycling for the other half. Fourier-transform infrared spectroscopy (FTIR) was performed to chemically analyze the remineralization, and the degree of nanoleakage in each sample was observed using a scanning electron microscope (SEM). The CPIC-incorporated PA-II solution decreased the nanoleakage in the hybrid layer without reducing the mu TBS, with or without thermocycling, and promoted remineralization of dentin collagen.

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