4.1 Article

Synthesis of 5,11-dialkyl-5,6,11,12-tetrahydro-6,12-epoxydibenzo[b,f][1,5]diazocines from 2-alkylaminobenzaldehydes

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CHEMISTRY OF HETEROCYCLIC COMPOUNDS
卷 58, 期 6-7, 页码 354-357

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SPRINGER
DOI: 10.1007/s10593-022-03097-4

关键词

2-alkylaminobenzaldehydes; tetrahydrodiazocines; Troger's base; acidic catalysis

资金

  1. Russian Science Foundation [20-73-10195]

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This methodology offers a straightforward approach to synthesize the targeted compound, which is achieved by reacting 2-alkylaminobenzaldehydes with hydrogen chloride solution in dioxane at room temperature.
A simple methodology was developed for the synthesis of 5,11-dialkyl-5,6,11,12-tetrahydro-6,12-epoxydibenzo[b,f][1,5]diazocines by treatment of the respective 2-alkylaminobenzaldehydes with hydrogen chloride solution in dioxane at room temperature.

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