High performance curcumin subcritical water extraction from turmeric (Curcuma longa L.)

Curcumin is a hydrophobic polyphenolic compound derived from turmeric rhizome, which consists about 2-5% of the total rhizome content and is a more valuable component of turmeric. For reducing the drawbacks of conventional extraction (using organic solvents) of curcumin, the water as a clean solvent was used for extracting curcumin. Subcritical water extraction (SWE) experimental setup was fabricated in a laboratory scale and the influences of some parameters (e.g. extraction temperature, particle size, retention time and pressure) on the yield of extraction were investigated. Optimum extraction conditions such as SWE pressure of 10 bar, extractive temperature of 140 degrees C, particle size of 0.71 mm and retention time of 14 min were defined. The maximum amount of curcumin extracted at the optimum condition was 3.8 wt%. The yield of curcumin extraction was more than 76 wt% with regards to the maximum possible curcumin content of turmeric, as known to be 5%. The scanning electron microscope (SEM) images from the outer surface of turmeric, before and after extraction, clearly demonstrated the effect of each parameter; changes in porosity and hardness of turmeric that is directly related to the amount of extracted curcumin in process optimization of the extraction parameters. (C) 2016 Elsevier B.V. All rights reserved.