期刊
JOURNAL OF CHROMATOGRAPHIC SCIENCE
卷 55, 期 3, 页码 373-377出版社
OXFORD UNIV PRESS INC
DOI: 10.1093/chromsci/bmw178
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A low-density polyethylene (LDPE) membrane pouch method was developed to extract volatile flavor compounds from tobacco leaf. Tobacco leaf suspended in water was enclosed in a pouch prepared from a LDPE membrane of specific gravity 0.92 g/cm(3) and 0.03mm thickness and then extracted with diethyl ether. In comparison with direct solvent extraction, LDPE membrane excluded larger and higher boiling point compounds which could contaminate a gas chromatograph inlet and damage a column. Whilst being more convenient than a reduced-pressure steam distillation, it could extract volatile flavor compounds of wide range of molecular weight and polarity. Repeatabilities in the extracted amounts were ranged from 0.38% of 2.3-bipyridyl to 26% of beta-ionone, and average value of 39 compounds was 5.9%.
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