期刊
JOURNAL OF CHEMICAL EDUCATION
卷 94, 期 1, 页码 79-84出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.jchemed.6b00355
关键词
Second-Year Undergraduate; Organic Chemistry; Analytical Chemistry; Laboratory Instruction; Hands-On Learning/Manipulatives; Computer-Based Learning; Stereochemistry; Chirality/Optical Activity; Enantiomers; NMR Spectroscopy
资金
- Royal Society
- EPSRC [EP/J003220/1]
- Welch Regents Chair [F-0046]
- University of Birmingham
- Royal Society of Chemistry
- Society for Chemical Industry
- Engineering and Physical Sciences Research Council [EP/J003220/1] Funding Source: researchfish
- EPSRC [EP/J003220/1] Funding Source: UKRI
An undergraduate chemistry experiment that draws from primary research is described. The experiment exploits chiral supramolecular assemblies for the determination of enantiomeric excess by H-1 NMR spectroscopy. This report describes the delivery of the experiment to a cohort of students, and as a result of feedback from those involved, an optimized protocol is presented. Particular care has been taken to facilitate ready adoption in other institutions by providing comprehensive teaching support materials as well as technical guidance-for supporting the experiment.
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