期刊
ACS OMEGA
卷 7, 期 15, 页码 12879-12890出版社
AMER CHEMICAL SOC
DOI: 10.1021/acsomega.2c00141
关键词
-
资金
- DFG
- KIT-Publication Fund of the Karlsruhe Institute of Technology
Various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole compounds derived from the [2.2]paracyclophane molecule were successfully synthesized starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were determined using NMR, mass spectrometry, infrared spectroscopy, and high-resolution mass spectrometry (HRMS). X-ray crystallography was used to further confirm the assigned structures.
The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure.
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