☆ 4.7 Review

The ten principles of green sample preparation

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2022)

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Green analytical chemistry metrics: A review

Muhammad Sajid et al.

Summary: Green analytical chemistry promotes environmentally friendly practices such as reducing the use of toxic chemicals, energy-efficient equipment, and minimizing waste generation. Various metrics have been developed to evaluate the greenness of analytical procedures, with tools like Analytical Eco-Scale and Green Analytical Procedure Index playing important roles in assessing the environmental impact of analytical processes. This paper explores the principles and applications of these greenness evaluation metrics, highlighting both their advantages and limitations in promoting sustainable analytical practices.

TALANTA (2022)

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To separate or not to separate: what is necessary and enough for a green and sustainable extraction of bioactive compounds from Brazilian citrus waste

Vania G. Zuin et al.

Summary: The increasing demand for chemicals from greener and more sustainable sources requires exploring techniques like utilizing bioactive chemicals from non-food biomass waste. In the case study of obtaining flavonoids from orange peel, microwave extraction was found to be the most efficient method. The chemical profiles of orange waste from different farming models emphasized the importance of this alternative natural product resource.

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Article Chemistry, Analytical

Electromembrane extraction using deep eutectic solvents as the liquid membrane

Frederik Andre Hansen et al.

Summary: This study investigated hydrophobic deep eutectic solvents as supported liquid membranes for electromembrane extraction, and found that mixtures of coumarin and thymol were efficient in extracting non-polar bases, non-polar acids, and polar bases. The SLMs with aromatic properties exhibited high hydrogen bonding capabilities, providing excellent clean-up efficiency with no matrix effects from plasma.

ANALYTICA CHIMICA ACTA (2021)

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Miniaturized analytical methods for determination of environmental contaminants of emerging concern e A review

Francisco Pena-Pereira et al.

Summary: This paper reviews miniaturized analytical methods for the determination of contaminants of emerging concern (CECs) in environmental samples, covering the importance of monitoring CECs, downsized sample preparation methods, microextraction techniques, and miniaturized analytical flow techniques.

ANALYTICA CHIMICA ACTA (2021)

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How Can Chemometrics Support the Development of Point of Need Devices?

Sara Tortorella et al.

Summary: This article highlights the importance of chemometric-based approaches in the development of portable devices, which can help reduce costs and increase efficiency.

ANALYTICAL CHEMISTRY (2021)

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Review Chemistry, Inorganic & Nuclear

Metal-organic framework-based sorbents in analytical sample preparation

Maryam Bazargan et al.

Summary: Metal-organic frameworks (MOFs) are considered as an important material class in analytical applications due to their unique properties. The current limitation of MOFs in separation field lies in their chemical and thermal stabilities, which can be enhanced by ligand modification or cooperative combination with other materials. The role and applications of MOFs as sorbents in sample preparation have been widely studied, offering new solutions for future analytical sample preparation problems.

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Deep eutectic solvents. The new generation of green solvents in analytical chemistry

Alvaro Santana-Mayor et al.

Summary: The development of sustainable chemistry has led to the emergence of new materials, with deep eutectic solvents (DESs) as a promising non-toxic alternative to toxic organic solvents, seeing a significant increase in their applications in analytical chemistry in recent years. The vast amount of information generated from studies associated with DESs needs continuous revision.

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Polyamide-coated wooden tips coupled to direct infusion mass spectrometry, a high throughput alternative for the determination of methadone, cocaine and methamphetamine in oral fluid

Jaime Millan-Santiago et al.

Summary: The use of natural materials such as wooden tips with a porous structure coated with nylon 6 is proposed for the extraction of drugs of abuse from oral fluid samples. This method allows for simultaneous extraction of multiple samples and provides high sample throughput with detection limits of 1.5 μg L-1 for methamphetamine. Precision values were better than 9.1%, 12.6%, and 18.2% for methadone, cocaine, and methamphetamine respectively, with an accuracy range from 86% to 103%.

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Arpana Agrawal et al.

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TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2021)

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White Analytical Chemistry: An approach to reconcile the principles of Green Analytical Chemistry and functionality

Pawel Mateusz Nowak et al.

Summary: The concept of White Analytical Chemistry (WAC) extends from Green Analytical Chemistry (GAC) with 12 WAC principles proposed as an alternative to the known 12 GAC principles. WAC considers key criteria affecting the quality of the method, including analytical and practical aspects, aiming for coherence and synergy of analytical, ecological, and practical attributes.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2021)

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Green analytical chemistry as an integral part of sustainable education development

Justyna Plotka-Wasylka et al.

Summary: Green chemistry and analytical chemistry play crucial roles in the field of chemistry and must adhere to the principles of sustainable development in order to have a real impact.

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Alternative and sustainable solvents for green analytical chemistry

Ombeline Claux et al.

Summary: Analytical chemistry heavily relies on solvents, usually petroleum-based, with hazardous effects. The ideal alternative solvents for analysis should have high selectivity, solvency, low toxicity, low environmental impacts, be easily biodegradable and obtained from renewable resources at a reasonable price. However, finding a solvent that meets all these requirements is a challenge, as the optimum solvent selection depends on various factors such as extraction procedure, analytical method, matrix, and target molecules. This opinion presents a snapshot of current knowledge on alternative and sustainable solvents in analytical laboratories, focusing on innovation and development of safe products and procedures.

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Unmodified cellulose filter paper, a sustainable and affordable sorbent for the isolation of biogenic amines from beer samples

M. C. Diaz-Linan et al.

Summary: Current trends in Green Analytical Chemistry focus on simplifying sample treatment, but food matrices are often too complex for direct analysis. Biogenic amines, formed naturally in food products, have health implications. This study simplified the extraction of biogenic amines from beer samples using laboratory filter paper and direct infusion mass spectrometry, leading to efficient analysis.

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Redefining dilute and shoot: The evolution of the technique and its application in the analysis of foods and biological matrices by liquid chromatography mass spectrometry

Brett Greer et al.

Summary: With laboratories seeking to expand analytical capabilities, there has been a shift towards generic sample clean-up techniques like dilute-and-shoot. This methodology is simple, versatile, and facilitates high sample throughput and analysis of various analyte classes.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2021)

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Greening sample preparation: An overview of cutting-edge contributions

Francisco Pena-Pereira et al.

Summary: This review examines cutting-edge advances in greener analytical methods for sample preparation, focusing on the use of environmentally friendly solvents and adsorbents, integration of unitary steps, miniaturization, and automation. The paper also addresses concluding remarks and additional considerations for further improvements.

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Complementary green analytical procedure index (ComplexGAPI) and software

Justyna Plotka-Wasylka et al.

Summary: The study proposed a new metric based on GAC attributes for evaluating the green nature of analytical procedures. This metric expands on the green analytical procedure index by adding additional fields related to processes performed before the analytical procedure, and was used to evaluate analytical protocols for determining pesticides in urine samples. It is expected to gain attention and acceptance from the chemical community.

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ANALYTICA CHIMICA ACTA (2020)

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Application of in vivo solid phase microextraction (SPME) in capturing metabolome of apple (Malus xdomestica Borkh.) fruit

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Giorgio Marrubini et al.

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Cotton fibers functionalized with β-cyclodextrins as selectivity enhancer for the direct infusion mass spectrometric determination of cocaine and methamphetamine in saliva samples

M. T. Garcia-Valverde et al.

ANALYTICA CHIMICA ACTA (2020)

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Elefteria Psillakis

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Solid-Phase Microextraction Fiber in Face Mask for in Vivo Sampling and Direct Mass Spectrometry Analysis of Exhaled Breath Aerosol

Zi-Cheng Yuan et al.

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AGREE-Analytical GREEnness Metric Approach and Software

Francisco Pena-Pereira et al.

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Online polymer monolith microextraction with in-situ derivatization for sensitive detection of endogenous brassinosteroids by LC-MS

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Ana Ballester-Caudet et al.

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Priscilla Rocio-Bautista et al.

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M. M. Delgado-Povedano et al.

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Coupling of two centrifugeless ultrasound-assisted dispersive solid/liquid phase microextractions as a highly selective, clean, and efficient method for determination of ultra-trace amounts of non-steroidal anti-inflammatory drugs in complicated matrices

Somayeh Arghavani-Beydokhti et al.

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Microwave-assisted digestion methods: towards greener approaches for plasma-based analytical techniques

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ANALYTICA CHIMICA ACTA (2016)

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Sampling-Rate Calibration for Rapid and Nonlethal Monitoring of Organic Contaminants in Fish Muscle by Solid-Phase Microextraction

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