4.5 Article

Fibrous nanosilica spheres KCC-1@NH2 as highly effective and easily retrievable catalyst for the synthesis of chromenes

期刊

RESEARCH ON CHEMICAL INTERMEDIATES
卷 48, 期 5, 页码 2069-2085

出版社

SPRINGER
DOI: 10.1007/s11164-022-04695-9

关键词

Fibrous nanosilica; Spheres; KCC-1; Chromenes; Multi-component

资金

  1. University of Kashan

向作者/读者索取更多资源

In this study, a three-component reaction was achieved using fibrous nanosilica spheres as catalysts to synthesize chromenes. The catalyst showed high surface area, stability, recyclability, and low toxicity, making it useful for the synthesis of chromenes. Characterization techniques including FT-IR, XRD, EDX, FE-SEM, TEM, BET, and TGA were used. The synthesized products were confirmed by H-1-NMR, C-13-NMR, and FT-IR.
A three-component reaction of naphthalene-1,5-diol, malononitrile and aromatic aldehydes has been achieved in the presence of fibrous nanosilica spheres KCC-1@NH2 as highly effective heterogeneous catalysts to produce of chromenes. In this study, simple and effective methods were used for the preparation of nanosilica spheres KCC-1@NH2 as basic catalysts. A fibrous surface morphology, high surface area, high mechanical stability, the easy separation of the nanocatalyst and the recyclability, nontoxicity, versatility, combined with low reaction times and excellent yields, make the present protocol very useful for the synthesis of the chromenes. The catalyst has been characterized by FT-IR, XRD, EDX, FE-SEM, TEM, BET and TGA. Also, the synthesized products were confirmed by H-1-NMR, C-13-NMR, FT-IR. [GRAPHICS] .

作者

我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。

评论

主要评分

4.5
评分不足

次要评分

新颖性
-
重要性
-
科学严谨性
-
评价这篇论文

推荐

暂无数据
暂无数据