4.8 Article

Total Synthesis of an All-1,2-cis-Linked Repeating Unit from the Acinetobacter baumannii D78 Capsular Polysaccharide

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ORGANIC LETTERS
卷 24, 期 19, 页码 3461-3465

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AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.2c01034

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  1. National Science Foundation [CHE-1665208, CHE-2101153]

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The assigned tetrasaccharide repeating subunit from the Acinetobacter baumannii KL4-associated capsular polysaccharide has been successfully synthesized through chemical synthetic efforts. A convergent synthetic strategy based on a 1,2-cis-selective [2+2] glycosylation was crucial for the synthesis of the fully protected tetrasaccharide.
Chemical synthetic efforts have resulted in the preparation of the assigned tetrasaccharide repeating subunit from the Acinetobacter baumannii KL4-associated capsular polysaccharide. A convergent synthetic strategy hinging on a 1,2-cis-selective [2+2] glycosylation to generate the fully protected tetrasaccharide was key to the success of this synthesis.

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