期刊
ORGANIC LETTERS
卷 24, 期 8, 页码 1747-1751出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.2c00430
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资金
- Ludwig-Maximilian University (LMU)
- Office of Naval Research (ONR) [ONR N00014-19-1-2078]
- Strategic Environmental Research and Development Program (SERDP) [W912HQ19C0033]
1,1'-Diamino-5,5'-bistetrazole is a highly nitrogen-containing compound with promising energetic characteristics. It can be synthesized through a classic organic reaction protocol, which is the only Krapcho reaction on a carbamate system described in the literature. Extensive characterization and demonstration of its capability to initiate PETN have been conducted.
1,1'-Diamino-5,5'-bistetrazole (C2H4N10), a highly nitrogen-containing compound with promising energetic characteristics, is available through a classic organic reaction protocol applied on an inorganic azole system. This is the only Krapcho reaction on a carbamate system described in the literature so far. 1,1'-Diamino-5,5'-bistetrazole was extensively characterized through multinuclear spectroscopy, mass spectrometry, thermal analysis, and X-ray diffraction. The sensitivity values were measured, and detonation values were calculated. Its capability to initiate pentaerythritol tetranitrate (PETN) was successfully demonstrated.
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