Achieving excellent mechanical properties in type 316 stainless steel by tailoring grain size in homogeneously recovered or recrystallized nanostructures

One hopeful path to realize good comprehensive mechanical properties in metallic materials is to accomplish homogeneous nanocrystalline (NC) or ultrafine grained (UFG) structure with low dislocation density. In this work, high pressure torsion deformation followed by appropriate annealing was performed on 316 stainless steel (SS). For the first time, we successfully obtained NC/UFG 316 SS having uniform microstructures with various average grain sizes ranging from 46 nm to 2.54 mu m and low dislocation densities. Dislocation scarcity in NC/UFG grains was found bringing significant extra enhancement in strength in addition to normal grain boundary hardening, which provided great freedom in tailoring mechanical property of the material with the wide range of average grain sizes. Among the series, an unprecedentedly high yield strength (2.34 GPa) was achieved at the smallest grain size of 46 nm, in which dislocation scarcity induced hardening accounting for 57% of the strength. On the other hand, exceptional strength-ductility synergy with high yield strength (900 MPa) and large uniform elongation (27%) was obtained in the fully recrystallized specimen having the grain size of 0.38 mu m, the finest recrystallized grain size ever reported. The high yield stress and scarcity of dislocation sources in recrystallized UFGs activated stacking faults and deformation twins nucleating from grain boundaries during straining, and their interaction with dislocations allowed for sustainable strain hardening, which also agreed with the plaston concept recently proposed. The multiple deformation modes activated, together with the effective strengthening mechanisms, were responsible for the outstanding comprehensive mechanical performance of the material.(c) 2022 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Automated summary

One way to achieve good comprehensive mechanical properties in metallic materials is to create a homogeneous nanocrystalline or ultrafine grained structure with low dislocation density. In this study, high pressure torsion deformation and annealing were used to obtain uniform microstructures with various grain sizes in 316 stainless steel. The scarcity of dislocations in the nanocrystalline/ultrafine grained regions resulted in significant enhancement in strength, in addition to the normal grain boundary hardening. The material exhibited outstanding mechanical performance, including high yield strength and exceptional strength-ductility synergy.