☆ 4.8 Review

Striding the threshold of an atom era of organic synthesis by single-atom catalysis

CHEM (2022)

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Confining isolated atoms and clusters in crystalline porous materials for catalysis

Lichen Liu et al.

Summary: This review discusses the impact of confining subnanometric metal species in zeolites and metal-organic frameworks on their geometric and electronic structures, as well as catalytic performance. It also highlights the potential of the interaction between metal species and porous frameworks in modulating the properties of subnanometric metal species. Future research directions in this area are proposed for further exploration.

NATURE REVIEWS MATERIALS (2021)

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Review Chemistry, Multidisciplinary

More is Different: Synergistic Effect and Structural Engineering in Double-Atom Catalysts

Yiran Ying et al.

Summary: Double-atom catalysts (DACs) have emerged as a novel frontier in heterogeneous catalysis, showing improved catalytic activity through synergistic effects while maintaining high atomic utilization efficiency, good selectivity, and stability. Current research focuses on the design, experimental and theoretical progress, and practical applications of DACs in various catalytic reactions.

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Article Nanoscience & Nanotechnology

A high-energy and long-cycling lithium-sulfur pouch cell via a macroporous catalytic cathode with double-end binding sites

Chen Zhao et al.

Summary: A novel cathode design for Li-S batteries utilizing single-atom Co catalyst and ZnS nanoparticles has successfully suppressed the shuttling effect, resulting in stable cycling and high energy performances.

NATURE NANOTECHNOLOGY (2021)

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Article Chemistry, Physical

Atmosphere-Pressure Methane Oxidation to Methyl Trifluoroacetate Enabled by a Porous Organic Polymer-Supported Single-Site Palladium Catalyst

Yiwen Zhang et al.

Summary: A porous organic polymer-supported Pd catalyst was reported, which can efficiently convert methane to a methanol precursor at 80 degrees Celsius under atmospheric pressure, with high catalytic activity and reusability for at least five runs. The catalyst has good affinity for methane uptake and homogeneous distribution of Pd2+ on the support, contributing to its high catalytic performance in methane conversion.

ACS CATALYSIS (2021)

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Article Chemistry, Multidisciplinary

Soluble/MOF-Supported Palladium Single Atoms Catalyze the Ligand-, Additive-, and Solvent-Free Aerobic Oxidation of Benzyl Alcohols to Benzoic Acids

Estefania Tiburcio et al.

Summary: Palladium single atoms can be spontaneously formed in neat benzyl alcohols and used for organic oxidation reactions without additives or solvents. By stabilizing Pd SACs within a metal-organic framework, a solid catalyst was successfully prepared and characterized.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2021)

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Review Chemistry, Multidisciplinary

Deciphering the Local Environment of Single-Atom Catalysts with X-ray Absorption Spectroscopy

Yuanyuan Li et al.

Summary: This article discusses strategies to enhance reactivity of catalysts by increasing the number of active sites and improving intrinsic activity per active site, emphasizing the impact of unique structures and interactions of single-atom catalysts (SACs) with supports on their reactivity. The study is important for addressing the complexity of catalytically active species distribution heterogeneity in SACs.

ACCOUNTS OF CHEMICAL RESEARCH (2021)

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Review Chemistry, Multidisciplinary

Zeolite Fixed Metal Nanoparticles: New Perspective in Catalysis

Yeqing Wang et al.

Summary: Loading metal nanoparticles within zeolite crystals provides advantages of high activity, shape selectivity, and stability, addressing the shortcomings of traditional supported metal nanoparticles. The combination of metal nanoparticles and zeolites in metal@zeolite catalysts offers enhanced catalytic performance by facilitating reactant diffusion, adjusting adsorption, and sieving reactants and products in zeolite micropores. Optimizing wettability and microporous confinement in zeolites further improves efficiency and productivity in catalytic reactions, making these catalysts promising for industrial applications and fundamental catalytic research.

ACCOUNTS OF CHEMICAL RESEARCH (2021)

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Isolated metal atoms and clusters for alkane activation: Translating knowledge from enzymatic and homogeneous to heterogeneous systems

Lichen Liu et al.

Summary: Activation of alkanes can be achieved with a variety of catalysts, including enzymes, homogeneous, and heterogeneous metal catalysts. Despite differences in catalyst structures and reaction conditions among the three catalysis fields, there are similarities in terms of active site structures and reaction mechanisms. Lessons learned from enzymatic and molecular catalysts can be applied to improve the understanding and development of heterogeneous metal catalysts for practical applications in alkane activation.

CHEM (2021)

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Accelerated Anti-Markovnikov Alkene Hydrosilylation with Humic-Acid-Supported Electron-Deficient Platinum Single Atoms

Kairui Liu et al.

Summary: The study synthesized electron-deficient Pt single atoms supported on humic matter for use as a catalyst in hydrosilylation reactions, demonstrating super activity and selectivity. Density functional theory calculations revealed the high performance was due to the atomic dispersion of Pt and electron deficiency of the Pt-1 atoms, different from traditional Pt nanoscale catalysts. The catalyst maintained excellent performance during recycle experiments, indicating high stability.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

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The Electronic Metal-Support Interaction Directing the Design of Single Atomic Site Catalysts: Achieving High Efficiency Towards Hydrogen Evolution

Jiarui Yang et al.

Summary: Catalysts designed by electronic metal-support interactions (EMSI), especially the single atomic site catalyst Rh1-TiC, show higher catalytic efficiency than Pt/C, with smaller overpotentials, lower Tafel slopes, and higher mass activities. Additionally, they demonstrate energy-saving advantages compared to Pt/C.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2021)

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Review Chemistry, Multidisciplinary

Chiral Tridentate Ligands in Transition Metal-Catalyzed Asymmetric Hydrogenation

Heng Wang et al.

Summary: Asymmetric hydrogenation of double bonds is an effective method for preparing chiral molecules, with noble metals and bidentate ligands showing remarkable reactivity. The development of chiral tridentate ligands has become increasingly important, enabling both reactivities and stereoselectivities in asymmetric hydrogenation. While noble metal catalysts with chiral tridentate ligands have made significant achievements, there is still a high demand for designing chiral tridentate ligands for earth abundant metal catalysts.

CHEMICAL REVIEWS (2021)

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Creating High Regioselectivity by Electronic Metal-Support Interaction of a Single-Atomic-Site Catalyst

Wen-Hao Li et al.

Summary: By designing and synthesizing a single-atomic-site catalyst with strong electronic metal-support interaction effects, researchers achieved highly selective conversion of electronically unbiased alkynes. Through studying reaction mechanisms, they demonstrated the exciting potential of EMSI in regulating regioselectivity in homogeneous catalysis.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2021)

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Phosphorus coordinated Rh single-atom sites on nanodiamond as highly regioselective catalyst for hydroformylation of olefins

Peng Gao et al.

Summary: Single-atom Rh catalysts show superior activity in olefins hydroformylation but limited success in regioselectivity control. By developing a Rh1 single-atom catalyst with nanodiamond as support, the catalyst achieved good to excellent regioselectivities in hydroformylation of arylethylenes, comparable to homogeneous counterparts. The coordination interaction between Rh-1 and surface phosphorus species was clarified by P-31 solid-state NMR and X-ray absorption spectroscopy.

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Article Chemistry, Physical

A heterogeneous iridium single-atom-site catalyst for highly regioselective carbenoid O-H bond insertion

Jie Zhao et al.

Summary: The strategy of selective carbenoid O-H insertion using an engineered heterogeneous iridium single-atom catalyst provides opportunities for organic transformations by merging material science and catalysis. This catalytic protocol delivers excellent selectivities for the functionalization of aliphatic over phenolic O-H bonds, showcasing a superior site-selectivity of a heterogeneous single-atom catalyst.

NATURE CATALYSIS (2021)

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Site-directed reduction engineering within bimetal-organic frameworks for efficient size-selective catalysis

Xiao-Jue Bai et al.

Summary: Directional reduction processing of MOFs has enabled the customization of hierarchical MOFs/metal nanoparticle composites with different structures, exhibiting unique size-selective catalytic properties.

MATTER (2021)

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Single-atom catalysis in advanced oxidation processes for environmental remediation

Yanan Shang et al.

Summary: Carbon-based single atom catalysts show high performances and efficiency in environmental catalysis, but there is a lack of comprehensive research on their catalytic sites and mechanisms in advanced oxidation processes, which is necessary for further exploration.

CHEMICAL SOCIETY REVIEWS (2021)

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Single-Atom Materials: Small Structures Determine Macroproperties

Jiarui Yang et al.

Summary: Single-atom materials (SAMs) have been widely studied in various fields, and their high performance is largely attributed to the microstructure inside the SAM. Achieving the goal of regulating structures and understanding the relationship between macroproperties and small structures are essential but require further efforts in this field. This review comprehensively summarizes and discusses the regulation on microstructures, the characterization of microstructures, and the relationship between macroproperties and small structures, mainly focusing on the application of SAM in catalysts. Proposed challenges and future developments aim to provide an overall view and guidance for future research in this area.

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Styrene Hydroformylation with In Situ Hydrogen: Regioselectivity Control by Coupling with the Low-Temperature Water-Gas Shift Reaction

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Stable single platinum atoms trapped in sub-nanometer cavities in 12CaO•7Al2O3 for chemoselective hydrogenation of nitroarenes

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Tuning Polarity of Cu-O Bond in Heterogeneous Cu Catalyst to Promote Additive-free Hydroboration of Alkynes

Jian Zhang et al.

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Nanostructuring unlocks high performance of platinum single-atom catalysts for stable vinyl chloride production

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Integration of Metal Single Atoms on Hierarchical Porous Nitrogen-Doped Carbon for Highly Efficient Hydrogenation of Large-Sized Molecules in the Pharmaceutical Industry

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ACS APPLIED MATERIALS & INTERFACES (2020)

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Chemical Synthesis of Single Atomic Site Catalysts

Shufang Ji et al.

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Carbon Nitride-Based Single-Atom Cu Catalysts for Highly Efficient Carboxylation of Alkynes with Atmospheric CO2

Peng Yang et al.

INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH (2020)

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Article Multidisciplinary Sciences

Strong metal-support interaction promoted scalable production of thermally stable single-atom catalysts

Kaipeng Liu et al.

NATURE COMMUNICATIONS (2020)

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Review Chemistry, Physical

Modulating the local coordination environment of single-atom catalysts for enhanced catalytic performance

Xinyuan Li et al.

NANO RESEARCH (2020)

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Single-Atom Alloy Catalysis

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Porous Ligand Creates New Reaction Route: Bifunctional Single-Atom Palladium Catalyst for Selective Distannylation of Terminal Alkynes

Wen-Yong Huang et al.

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Iridium single-atom catalyst on nitrogen-doped carbon for formic acid oxidation synthesized using a general host-guest strategy

Zhi Li et al.

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Electrocatalysis of Single-Atom Sites: Impacts of Atomic Coordination

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Electronic Metal-Support Interaction of Single-Atom Catalysts and Applications in Electrocatalysis

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Palladium Nanoparticles on Assorted Nanostructured Supports: Applications for Suzuki, Heck, and Sonogashira Cross-Coupling Reactions

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Atomically Dispersed Ruthenium Species Inside Metal-Organic Frameworks: Combining the High Activity of Atomic Sites and the Molecular Sieving Effect of MOFs

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Zeolite-Encaged Single-Atom Rhodium Catalysts: Highly-Efficient Hydrogen Generation and Shape-Selective Tandem Hydrogenation of Nitroarenes

Qiming Sun et al.

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Constructing Mononuclear Palladium Catalysts by Precoordination/Solvothermal Polymerization: Recyclable Catalyst for Regioselective Oxidative Heck Reactions

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Chuan-Ming Wang et al.

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Control of metal-support interactions in heterogeneous catalysts to enhance activity and selectivity

Tom W. van Deelen et al.

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Maximizing the Number of Interfacial Sites in Single-Atom Catalysts for the Highly Selective, Solvent-Free Oxidation of Primary Alcohols

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Pd Metal Catalysts for Cross-Couplings and Related Reactions in the 21st Century: A Critical Review

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Discovering Partially Charged Single-Atom Pt for Enhanced Anti-Markovnikov Alkene Hydrosilylation

Yuanjun Chen et al.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2018)

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Single-site catalyst promoters accelerate metal-catalyzed nitroarene hydrogenation

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Cation vacancy stabilization of single-atomic-site Pt-1/Ni(OH)(x) catalyst for diboration of alkynes and alkenes

Jian Zhang et al.

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JOURNAL OF MATERIALS CHEMISTRY A (2018)

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Design of Effective Catalysts for Selective Alkyne Hydrogenation by Doping of Ceria with a Single-Atom Promotor

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Xantphos doped Rh/POPs-PPh3 catalyst for highly selective long-chain olefins hydroformylation: Chemical and DFT insights into Rh location and the roles of Xantphos and PPh3

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Performance of Cu-Alloyed Pd Single-Atom Catalyst for Semihydrogenation of Acetylene under Simulated Front-End Conditions

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Single atom dispersed Rh-biphephos&PPh3@porous organic copolymers: highly efficient catalysts for continuous fixed-bed hydroformylation of propene

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Photochemical route for synthesizing atomically dispersed palladium catalysts

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Single-atom dispersed Co-N-C catalyst: structure identification and performance for hydrogenative coupling of nitroarenes

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Atomic-level insights in optimizing reaction paths for hydroformylation reaction over Rh/CoO single-atom catalyst

Liangbing Wang et al.

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A Stable Single-Site Palladium Catalyst for Hydrogenations

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Highly Efficient Heterogeneous Hydroformylation over Rh-Metalated Porous Organic Polymers: Synergistic Effect of High Ligand Concentration and Flexible Framework

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Privileged Phosphine-Based Metal-Organic Frameworks for Broad-Scope Asymmetric Catalysis

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