4.3 Article

Small-angle scattering for beginners

期刊

JOURNAL OF APPLIED CRYSTALLOGRAPHY
卷 54, 期 -, 页码 1832-1843

出版社

INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600576721010293

关键词

small-angle scattering; SAXS; SANS; form factors; structure factors

资金

  1. Fonds de la Recherche Scientifique -FNRS

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The article discusses the importance of small-angle scattering in analyzing nanostructures, pointing out that under stringent experimental conditions, SAS is often the only option. The rapid development of synchrotron and neutron facilities globally has opened up new possibilities for using SAS, but this method is still not covered enough in teaching.
Many experimental methods are available for the characterization of nanostructures, but most of them are limited by stringent experimental conditions. When it comes to analysing nanostructures in the bulk or in their natural environment - even as ordinary as water at room temperature - small-angle scattering (SAS) of X-rays or neutrons is often the only option. The rapid worldwide development of synchrotron and neutron facilities over recent decades has opened unprecedented possibilities for using SAS in situ and in a time-resolved way. But, in spite of its huge potential in the field of nanomaterials in general, SAS is covered far less than other characterization methods in nonspecialized curricula. Presented here is a rigorous discussion of small-angle scattering, at a technical level comparable to the classical undergraduate coverage of X-ray diffraction by crystals and which contains diffraction as a particular case.

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