4.7 Article

Neutron imaging of an operational dilution refrigerator

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SCIENTIFIC REPORTS
卷 12, 期 1, 页码 -

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NATURE PORTFOLIO
DOI: 10.1038/s41598-022-05025-0

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  1. ISIS cryogenics team

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The invention of the He-3/He-4 dilution refrigerator has greatly advanced experimental ultra-low temperature physics. Dilution refrigerators are crucial for creating ultra-low temperature environments for various experiments. The development of dilution refrigeration technology relies on a thorough understanding of the quantum mechanical processes in liquid helium at ultra-low temperatures. In this study, the researchers used neutron radiography to directly observe the operational dilution refrigerator, providing important insights into its behavior and failure modes. This method has the potential to significantly contribute to the research and development of advanced dilution refrigerators.
The invention of the He-3/He-4 dilution refrigerator opened a new chapter in experimental ultra-low temperature physics. Dilution refrigerators became essential for providing ultra-low temperature environments for nuclear demagnetisation experiments, superconducting-qubit quantum processors and highly sensitive bolometers used in fundamental physics experiments. Development of dilution refrigeration technology requires thorough understanding of the quantum mechanical processes that take place in liquid helium at ultra-low temperatures. For decades the quantum fluids research community provided valuable information to engineers and designers involved in the development of advanced dilution refrigerators. However, the lack of methods that allow the measurement of physical parameters of liquid helium during the operation of a dilution refrigerator was hindering development of the technology. Here we show direct imaging of an operational dilution refrigerator using neutron radiography. This allows direct observation of the dilution process in He-3/He-4 mixtures and opens an opportunity for direct measurement of the He-3 concentration. We observe the refrigerator behaviour in different regimes, such as continuous circulation and single shot, and show that our method allows investigation of various failure modes. Our results demonstrate that neutron imaging applied to the study of dilution refrigeration processes can provide essential information for developers of ultra-low temperature systems. We expect that neutron imaging will become instrumental in the research and development of advanced dilution refrigerators.

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