☆ 4.8 Review

Revisiting the Preparation Progress of Nano-Structured Si Anodes toward Industrial Application from the Perspective of Cost and Scalability

ADVANCED ENERGY MATERIALS (2022)

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Summary: Silicon has garnered attention for its high specific capacity and abundant reserves, but its volumetric changes during charging and discharging processes have hindered industrial utilization. This study introduces a novel hybrid anode material, Si@void/CNF, designed with a nodes-connected structure that provides both a conductive reticulation for silicon nanoparticles and addresses volume variation. By adjusting the mass ratio of silicon to PMMA, an optimal structure was achieved, demonstrating excellent electrochemical performance with high specific capacity and cycling stability. The electrospun structure of nodes-connected Si@void/CNF offers a promising method for fabricating advanced silicon-based anode materials.

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Carbon dioxide solid-phase embedding reaction of silicon-carbon nanoporous composites for lithium-ion batteries

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Summary: This study prepared an in-situ doped Si/carbon anode material using SiO2 and CO2 as raw materials, achieving nanosizing of silicon and construction of a 3D carbon network, which improved electrical conductivity and cycling performance of the battery. The simple preparation method provides a new idea for modifying silicon-based anode materials, offering valuable insights for further research on carbon doping.

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Low-temperature and high-performance Si/graphite composite anodes enabled by sulfite additive

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Summary: This research introduces an electrolyte additive that enhances the performance and cycle life of Si/graphite composite anodes, improving low-temperature performance by introducing a high-ductility organic/inorganic solid electrolyte interface layer and promoting rapid defluorination of Fluoroethylene carbonate (FEC) and formation of organic layer. This study provides a practical method to enhance the performance of lithium-ion batteries in cold climates and shows a path for commercial LIBs to operate effectively in such conditions.

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Article Chemistry, Physical

Boosting anode performance of mesoporous Si by embedding copper nano-particles

Yao Zhang et al.

Summary: Embedding Cu nano-particles into mesoporous Si significantly improved the cycle stability and rate capability of the Si anode for lithium-ion batteries. The Cu nano-particles played dual roles in supporting the Si structure to prevent fracture and providing a pathway for enhanced mass transportation, resulting in improved lithium diffusion coefficient and charge transfer rate.

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Electrochemically induced high ion and electron conductive interlayer in porous multilayer Si film anode with enhanced lithium storage properties

Qiulin Chen et al.

Summary: By constructing Zn/Si/ZnO porous multi-layer film anodes, the specific capacity and cycling performance of lithium ion batteries have been significantly improved, thanks to the design of porous and multilayer structure and the formation of 3D conductive channels from Li-Zn alloy during cycling.

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Direct Growth of Si, Ge, and Si-Ge Heterostructure Nanowires Using Electroplated Zn: An Inexpensive Seeding Technique for Li-Ion Alloying Anodes

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Summary: The study describes a method of electroplating metallic Zn seeds on stainless steel substrates to grow Si and Ge nanowires. The use of Zn as a catalyst produces defect-rich Si NWs with high discharge capacity and stable cycling performance. The Zn seeds actively participate in Li-cycling activities, resulting in a highly porous network structure for improved performance.

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The robust carbon shell to improve stability of porous Si anodes for high-performance lithium-ion batteries

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Summary: The carbon-coated porous silicon (P-Si@C) materials showed improved performance in lithium-ion batteries, with porous structure mitigating silicon expansion and robust carbon shell enhancing overall electrical conductivity. This led to a high initial Coulombic efficiency and long cycle life, demonstrating potential for high capacity and stability in LIBs.

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Summary: A localized high-concentration electrolyte was designed for silicon anodes to enhance cycling stability over a wide temperature range, showing potential for improved battery performance. Full cells using this electrolyte retained 80% capacity after 500 cycles, demonstrating enhanced thermal stability. The electrolyte design principles developed in this study can be applied to extend the cycle life of other high-capacity electrode materials.

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A Ge/Carbon Atomic-Scale Hybrid Anode Material: A Micro-Nano Gradient Porous Structure with High Cycling Stability

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Summary: By selecting a suitable carbon source and introducing an active medium, Ge/carbon doping at the atom level was achieved, leading to excellent electrochemical performance. The Ge/carbon anode maintained a reversible capacity of 1127 mAh g(-1) after 1000 cycles with a retention of 84% compared to the second cycle, while the SEI thickness was only 17.4 nm after 1000 cycles, reflecting the material's application potential.

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Facile and Efficient Fabrication of Branched Si@C Anode with Superior Electrochemical Performance in LIBs

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Summary: The novel branched Si architecture fabricated through laser processing and dealloying showed improved area capacity and cycling stability. The branched Si@C anode demonstrated high gravimetric capacity and good retention rates at different cycling rates. This study highlights the importance of dendritic microstructure in the fabrication of branched Si and provides new insights into efficient fabrication of Si nanostructures.

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Summary: The use of free-standing Si/C-ZIF-8/CNFs electrodes can achieve high capacity and good cycling performance. This study provides a new pathway for the development of high-performance silicon-based anodes.

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Summary: The study demonstrates a novel interconnected hollow Si/C nanospheres with thin shells consisting of Si crystals and highly wrinkled amorphous carbon layers, synthesized by introducing CO2 as a green carbon source in magnesiotherimic reduction to accelerate commercial application. The interconnected carbon networks and MgO cores are simultaneously generated via the reaction between CO2 and excess Mg vapor, with the hollow structure realized after removing in-situ generated MgO templates through acid etching. The unique interconnected Si/C hybrid delivers high capacity, impressive cycling performance, and good Coulombic efficiency, benefiting from improved Li+ ion transportation and electron transfer kinetics, as well as the volume buffering effects of the hollow architecture.

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Summary: A scalable method was developed to synthesize nanoporous Si using Al-Si-Ni amorphous precursor alloys, with controlled pore and ligament sizes. The Ni-coated nanoporous Si showed high initial coulombic efficiency and high reversible capacity after 500 cycles, indicating its potential as a novel strategy for next-generation LIBs.

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ACS ENERGY LETTERS (2021)

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Tailoring Stress and Ion-Transport Kinetics via a Molecular Layer Deposition-Induced Artificial Solid Electrolyte Interphase for Durable Silicon Composite Anodes

Jia-Bin Fang et al.

Summary: This study explores the use of titanicone coating prepared by molecular layer deposition as a solid electrolyte interphase layer for silicon anodes, aiming to enhance the performance of lithium-ion batteries. The optimized titanicone-coated anode shows high cycling stability and excellent rate performance, indicating the potential for next-generation lithium-ion batteries.

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Composite Separators for Robust High Rate Lithium Ion Batteries

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Summary: Composite separators play a crucial role in improving the thermal stability, mechanical strength, electrolyte uptake, and ionic conductivity of lithium ion batteries.

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Functionalization-assistant ball milling towards Si/graphene anodes in high performance Li-ion batteries

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Summary: The paper presents a cost-effective method for synthesizing Si and graphene composites through ball-milling, demonstrating their outstanding performance in lithium-ion batteries and potential for large-scale production in the future.

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Novel silicon/copper nanowires as high-performance anodes for lithium ion batteries

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Summary: Si/Cu/Zn ternary microspheres are prepared by a pulsed electrical discharging method, with Zn and partial Si selectively removed to form Si/Cu nanowires. The nanowires exhibit high discharge capacity and cycling performance, attributed to the conductive Cu network and nanowire structure. The anode utilizes cheap materials and flexible processing methods，promising to boost the yield of Si alloy NWs with low cost.

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Article Chemistry, Physical

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Si/C particles on graphene sheet as stable anode for lithium-ion batteries

Jian Han et al.

Summary: In this work, a Si/C structure on graphene sheets was obtained to address the issue of large volume expansion during lithiation of silicon, showing improved cycling and rate performance. The Si/C-G anode materials exhibited high reversible capacity and good rate capability, significantly enhancing the commercial viability of silicon electrodes in high-energy-density LIBs.

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Spontaneous formation of the conformal carbon nanolayer coated Si nanostructures as the stable anode for lithium-ion batteries from silica nanomaterials

Xi Huang et al.

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JOURNAL OF POWER SOURCES (2021)

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Review Green & Sustainable Science & Technology

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Summary: This article reviews the current status and challenges of echelon utilization for retired lithium batteries, comprehensively summarizes the standards, policies, technologies, and environmental values of echelon utilization, and provides valuable solutions to address technical issues.

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SiOx Anode: From Fundamental Mechanism toward Industrial Application

Haoyu Li et al.

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SMALL (2021)

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Reversible oxide formation during cycling of Si anodes

Tobias Kohler et al.

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Philipp Gribisch et al.

Summary: The structural and morphological properties of gadolinium oxide (Gd2O3) grown at high temperatures with molecular beam epitaxy on Si(001) were investigated for different stages of growth. The results suggest that the nanowire-like structures on Si(001) substrates have specific orientations, and the density and length can be tuned by changing the oxygen partial pressure.

RSC ADVANCES (2021)

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Nanoporous noble metal-based alloys: a review on synthesis and applications to electrocatalysis and electrochemical sensing

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High-performance silicon-carbon anode material via aerosol spray drying and magnesiothermic reduction

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NANO ENERGY (2019)

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Particle size optimization enabled high initial coulombic efficiency and cycling stability of micro-sized porous Si anode via AlSi alloy powder etching

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ELECTROCHIMICA ACTA (2019)

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Scalable Engineering of Bulk Porous Si Anodes for High Initial Efficiency and High-Areal-Capacity Lithium-Ion Batteries

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Life Cycle Assessment of Silicon-Nanotube-Based Lithium Ion Battery for Electric Vehicles

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Multi-core yolk-shell like mesoporous double carbon-coated silicon nanoparticles as anode materials for lithium-ion batteries

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Achieving high energy density for lithium-ion battery anodes by Si/C nanostructure design

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Laser Porosificated Silicon Anodes for Lithium Ion Batteries

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ADVANCED ENERGY MATERIALS (2018)

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Efficient Sodium Storage in Rolled-Up Amorphous Si Nanomembranes

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Ionically Conductive Self-Healing Binder for Low Cost Si Microparticles Anodes in Li-Ion Batteries

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SCIENTIFIC REPORTS (2018)

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Boron-doped porous Si anode materials with high initial coulombic efficiency and long cycling stability

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JOURNAL OF MATERIALS CHEMISTRY A (2018)

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Continuous silicon oxycarbide fiber mats with tin nanoparticles as a high capacity anode for lithium-ion batteries

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SUSTAINABLE ENERGY & FUELS (2018)

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An amorphous Si material with a sponge-like structure as an anode for Li-ion and Na-ion batteries

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NANOSCALE (2018)

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NATURE COMMUNICATIONS (2018)

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A review of magnesiothermic reduction of silica to porous silicon for lithium-ion battery applications and beyond

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A mini-review on the development of Si-based thin film anodes for Li-ion batteries

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MATERIALS TODAY ENERGY (2018)

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Self-Templating Construction of 3D Hierarchical Macro-/Mesoporous Silicon from OD Silica Nanoparticles

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Self-standing silicon-carbon nanotube/graphene by a scalable in situ approach from low-cost Al-Si alloy powder for lithium ion batteries

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Conductive and Porous Silicon Nanowire Anodes for Lithium Ion Batteries

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Vertical Graphene Growth on SiO Microparticles for Stable Lithium Ion Battery Anodes

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Nanosilicon anodes for high performance rechargeable batteries

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Cost-effective approach for structural evolution of Si-based multicomponent for Li-ion battery anodes

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Room-Temperature Solution Synthesis of Mesoporous Silicon for Lithium Ion Battery Anodes

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Tunable Synthesis of Yolk-Shell Porous Silicon@Carbon for Optimizing Si/C-Based Anode of Lithium-Ion Batteries

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High-Rate and Long-Cycle Silicon/Porous Nitrogen-Doped Carbon Anode via a Low-Cost Facile Pre-Template-Coating Approach for Li-ion Batteries

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ELECTROCHIMICA ACTA (2017)

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Mesoporous Silicon Hollow Nanocubes Derived from Metal-Organic Framework Template for Advanced Lithium-Ion Battery Anode

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Protecting Silicon Film Anodes in Lithium-Ion Batteries Using an Atomically Thin Graphene Drape

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Enhanced Electrochemical Performance of Heterogeneous Si/MoSi2 Anodes Prepared by a Magnesiothermic Reduction

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Free-Standing Si/Graphene Paper Using Si Nanoparticles Synthesized by Acid-Etching Al-Si Alloy Powder for High-Stability Li-Ion Battery Anodes

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Failure mechanisms of single-crystal silicon electrodes in lithium-ion batteries

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NATURE COMMUNICATIONS (2016)

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Carbon-coated mesoporous silicon microsphere anodes with greatly reduced volume expansion

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Scalable production of 3D plum-pudding-like Si/C spheres: Towards practical application in Li-ion batteries

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NANO ENERGY (2016)

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Free-Standing Graphene-Encapsulated Silicon Nanoparticle Aerogel as an Anode for Lithium Ion Batteries

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CHEMNANOMAT (2016)

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Scalable synthesis of silicon-nanolayer-embedded graphite for high-energy lithium-ion batteries

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NATURE ENERGY (2016)

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Growth of conformal graphene cages on micrometre-sized silicon particles as stable battery anodes

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In-situ synthesis of interconnected SWCNT/OMC framework on silicon nanoparticles for high performance lithium-ion batteries

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GREEN ENERGY & ENVIRONMENT (2016)

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One-Step Synthesis of Si@C Nanoparticles by Laser Pyrolysis: High-Capacity Anode Material for Lithium-Ion Batteries

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Porous Si Nanowires from Cheap Metallurgical Silicon Stabilized by a Surface Oxide Layer for Lithium Ion Batteries

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Scalable Production of Si Nanoparticles Directly from Low Grade Sources for Lithium-Ion Battery Anode

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Metal-assisted chemical etching of silicon and the behavior of nanoscale silicon materials as Li-ion battery anodes

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Scalable synthesis of highly dispersed silicon nanospheres by RF thermal plasma and their use as anode materials for high-performance Li-ion batteries

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Micro-sized nano-porous Si/C anodes for lithium ion batteries

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NANO ENERGY (2015)

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Stable Silicon Anodes for Lithium-Ion Batteries Using Mesoporous Metallurgical Silicon

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ADVANCED ENERGY MATERIALS (2015)

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Well dispersed silicon nanospheres synthesized by RF thermal plasma treatment and their high thermal conductivity and dielectric constant in polymer nanocomposites

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A 12%-Efficient Upgraded Metallurgical Grade Silicon-Organic Heterojunction Solar Cell Achieved by a Self-Purifying Process

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Identifying Crystallization- and Incorporation-Limited Regimes during Vapor-Liquid-Solid Growth of Si Nanowires

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Edge-Selectively Halogenated Graphene Nanoplatelets (XGnPs, X = Cl, Br, or I) Prepared by Ball-Milling and Used as Anode Materials for Lithium-Ion Batteries

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Flexible and Stretchable Lithium-Ion Batteries and Supercapacitors Based on Electrically Conducting Carbon Nanotube Fiber Springs

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From Si wafers to cheap and efficient Si electrodes for Li-ion batteries

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High performance amorphous-Si@SiOx/C composite anode materials for Li-ion batteries derived from ball-milling and in situ carbonization

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High-Density Silicon Nanowires Prepared via a Two-Step Template Method

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Bulk-Nanoporous-Silicon Negative Electrode with Extremely High Cyclability for Lithium-Ion Batteries Prepared Using a Top-Down Process

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A pomegranate-inspired nanoscale design for large-volume-change lithium battery anodes

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High-rate lithiation-induced reactivation of mesoporous hollow spheres for long-lived lithium-ion batteries

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Review Chemistry, Physical

Silicon-Based Nanomaterials for Lithium-Ion Batteries: A Review

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Facile synthesis of carbon decorated silicon nanotube arrays as anode material for high-performance lithium-ion batteries

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A low-cost and high performance ball-milled Si-based negative electrode for high-energy Li-ion batteries

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Intercalated Si/C films as the anode for Li-ion batteries with near theoretical stable capacity prepared by dual plasma deposition

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Facile Synthesis of Free-Standing Silicon Membranes with Three-Dimensional Nanoarchitecture for Anodes of Lithium Ion Batteries

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Stable Li-ion battery anodes by in-situ polymerization of conducting hydrogel to conformally coat silicon nanoparticles

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Up-scalable and controllable electrolytic production of photo-responsive nanostructured silicon

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Size-Dependent Fracture of Silicon Nanoparticles During Lithiation

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Designing nanostructured Si anodes for high energy lithium ion batteries

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Stable cycling of double-walled silicon nanotube battery anodes through solid-electrolyte interphase control

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Unveiling the Formation Pathway of Single Crystalline Porous Silicon Nanowires

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Dependence of Milling Time on Electrochemical Properties of Nano Si Electrodes Prepared by Ball-Milling

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JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY (2011)

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A review of the electrochemical performance of alloy anodes for lithium-ion batteries

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Formation of Si Nanowires by Direct Electrolytic Reduction of Porous SiO2 Pellets in Molten CaCl2

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JOURNAL OF THE ELECTROCHEMICAL SOCIETY (2011)

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Mesoporous Silicon Anodes Prepared by Magnesiothermic Reduction for Lithium Ion Batteries

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JOURNAL OF THE ELECTROCHEMICAL SOCIETY (2011)

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Size-dependent fracture of Si nanowire battery anodes

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JOURNAL OF THE MECHANICS AND PHYSICS OF SOLIDS (2011)

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Interconnected Silicon Hollow Nanospheres for Lithium-Ion Battery Anodes with Long Cycle Life

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NANO LETTERS (2011)

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Highly Interconnected Si Nanowires for Improved Stability Li-Ion Battery Anodes

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Solution-Grown Silicon Nanowires for Lithium-Ion Battery Anodes

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A Critical Size of Silicon Nano-Anodes for Lithium Rechargeable Batteries

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Lithium Insertion In Silicon Nanowires: An ab Initio Study

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NANO LETTERS (2010)

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Arrays of Sealed Silicon Nanotubes As Anodes for Lithium Ion Batteries

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Electrochemical preparation of silicon nanowires from nanometre silica in molten calcium chloride

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Carbon-Silicon Core-Shell Nanowires as High Capacity Electrode for Lithium Ion Batteries

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Silicon Nanotube Battery Anodes

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NANO LETTERS (2009)

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Three-Dimensional Porous Silicon Particles for Use in High-Performance Lithium Secondary Batteries

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Silicon nanowires as negative electrode for lithium-ion microbatteries

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Fabrication of silicon nanowire arrays with controlled diameter, length, and density

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Large-scale Si1-xGex quantum dot arrays fabricated by templated catalytic etching

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Amorphous silicon anode for lithium-ion rechargeable batteries

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High performance silicon nanowire field effect transistors

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Solution reduction synthesis of surface stabilized silicon nanoparticles

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CHEMICAL COMMUNICATIONS (2002)

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Silicon nanowires: Preparation, device fabrication, and transport properties

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