期刊
SYNTHETIC COMMUNICATIONS
卷 52, 期 2, 页码 185-189出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2021.2008449
关键词
Amine borane complex; hydrazines; reduction
资金
- National Institute for General Medical Science [GM11694]
The study showed that primary amine borane complexes are highly effective in reducing N,N-dimethylhydrazones, yielding the corresponding air-sensitive hydrazine products in excellent yields with as little as 1.1 equivalents.
A convenient method for the reduction of N,N-dimethylhydrazones using amine borane complexes generated in situ is described. It was found that primary amine borane complexes performed exceedingly well at reducing N,N-dimethylhydrazones in as little as 1.1 equivalents, furnishing the corresponding air-sensitive hydrazine products in excellent yields.
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