4.3 Article

Efficient reductions of dimethylhydrazones using preformed primary amine boranes

期刊

SYNTHETIC COMMUNICATIONS
卷 52, 期 2, 页码 185-189

出版社

TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2021.2008449

关键词

Amine borane complex; hydrazines; reduction

资金

  1. National Institute for General Medical Science [GM11694]

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The study showed that primary amine borane complexes are highly effective in reducing N,N-dimethylhydrazones, yielding the corresponding air-sensitive hydrazine products in excellent yields with as little as 1.1 equivalents.
A convenient method for the reduction of N,N-dimethylhydrazones using amine borane complexes generated in situ is described. It was found that primary amine borane complexes performed exceedingly well at reducing N,N-dimethylhydrazones in as little as 1.1 equivalents, furnishing the corresponding air-sensitive hydrazine products in excellent yields.

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