4.8 Article

Direct Hydrodecarboxylation of Aliphatic Carboxylic Acids: Metal- and Light-Free

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ORGANIC LETTERS
卷 24, 期 2, 页码 686-691

出版社

AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.1c04079

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  1. Engineering and Physical Sciences Research Council
  2. Syngenta [EP/L016419/1]
  3. AstraZeneca [EP/V519522/1]
  4. CRITICAT Centre for Doctoral Training
  5. Heriot-Watt University

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A mild and inexpensive method for direct hydrodecarboxylation of aliphatic carboxylic acids has been developed, which does not require metals, light, or catalysts, making the protocol operationally simple and more sustainable.
A mild and inexpensive method for direct hydrodecarboxylation of aliphatic carboxylic acids has been developed. The reaction does not require metals, light, or catalysts, rendering the protocol operationally simple, easy to scale, and more sustainable. Crucially, no additional H atom source is required in most cases, while a broad substrate scope and functional group tolerance are observed.

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