4.6 Article

Surface residual stress in amorphous SiO2 insulating layer on Si substrate near a Cu through-silicon via (TSV) investigated by nanoindentation

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ELSEVIER SCI LTD
DOI: 10.1016/j.mssp.2021.106153

关键词

Nanoindentaion; Surface residual stress; Through silicon via; Copper; Microstructure; Amorphous SiO2

资金

  1. Samsung Electronics
  2. KEIT program - Ministry Trade, Industry and Energy (MOTIE, Korea) [20010448]
  3. Korea Evaluation Institute of Industrial Technology (KEIT) [20010448] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)

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The distribution of residual stress in through-silicon vias (TSVs) during manufacture can be measured using nanoindentation, with the stress increasing due to post-heat treatments and higher current density during TSV electroplating.
Thermomechanical reliability remains challenging in through-silicon via (TSV) manufacture, a key technology in three-dimensional packaging of integrated circuits. A primary issue in reliability is the residual stress created during manufacture and operation by mismatch in thermal expansion coefficients of Cu, the TSV filling material, with surrounding materials. Nanoindentation is suggested as a tool to measure the distribution of residual stress in the amorphous top layer near Cu TSVs. Formation of Cu TSV generates the tensile residual stress in the vicinity of the TSVs, and the maximum residual stress in top SiO2 insulating layer is 322 MPa. The residual stress increases as 652 MPa by post-heat treatments, and increases as 390 MPa for higer current density of TSVs electroplating.

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