期刊
出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2021.142370
关键词
Recrystallization; Ni-Co-Based superalloy; Directional solidification; Constitutive equation; Microstructural evolution
类别
资金
- National Key R&D Program of China [2019YFA0705304, 2017YFA0700703]
- National Science and Technology Major Project of China
- IMR Innovation Fund [2021-PY09]
- Doctoral Start-up Foundation of Liaoning Province
This study investigated the deformation mechanisms and hot compression behaviors of a Ni-Co-based superalloy prepared using directional solidification. The effects of temperature and strain rate on dynamic recrystallization were analyzed, and constitutive equations were established. The dominant deformation mechanisms were found to be dependent on the strain rate and temperature.
In this work, hot compression behaviors and deformation mechanisms of a Ni-Co-based superalloy prepared using directional solidification (DS) were investigated by carrying out the isothermal compression tests within the temperature range of 1080-1190 degrees C and the strain rate range of 0.001-1 s(-1) under the true strain of 0.693. The effects of temperature and strain rate on dynamic recrystallization (DRX) were analyzed, and constitutive equations were established. The activation energies for gamma+gamma' dual-phase and the gamma single-phase regions of Ni-Co-based superalloy with columnar grains were 1190 kJ mol(-1) and 415 kJ mol(-1), respectively. The results showed that the dominant deformation mechanisms were closely related to the strain rate and temperature. DRX was accelerated at low strain rate conditions, while the DRX process was apparently sluggish at strain rates higher than 1 s(-1). The undissolved gamma' phase interacted with dislocations and accelerated the DRX of the matrix during gamma' sub-solvus temperature (1080-1120 degrees C) deformation. Continuous dynamic recrystallization (CDRX) nucleation proved to play a dominant role. During gamma' super-solvus temperature (1150-1190 degrees C) deformation, the dominant dynamic softening mechanism of the alloy is discontinuous dynamic recrystallization (DDRX). Local migration of grain boundaries (GBs) causes an increase of misorientation within the deformed grains and induced the formation of subgrain boundaries near the GBs, which subsequently evolved into high angle grain boundaries (HAGBs) and participated in DDRX. Furthermore, during high-temperature deformation in Ni-Co-based super alloys, the relatively rare microtwins (MTs) were detected under compression at 1100 degrees C/1 s(-1).
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