4.7 Article

On the isothermal sintering behavior and transparency of glass powders

期刊

JOURNAL OF NON-CRYSTALLINE SOLIDS
卷 571, 期 -, 页码 -

出版社

ELSEVIER
DOI: 10.1016/j.jnoncrysol.2021.121024

关键词

Boro-alumino-silicate glass; Isothermal sintering; Translucency

资金

  1. Key R&D plan of Shandong Province [2019GGX102007]
  2. Shandong Provincial Major Scientific and Technological Innovation Project, China [2019JZZY010357]
  3. Colleges and Universities Twenty Terms Foundation of Jinan City [2019GXRC034]
  4. Taishan Young Scholarship Project of Shandong Province [tsqn202103098]

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The study reveals that increasing sintering temperature can significantly enhance densification, while relatively high translucency can be achieved in conditions with low crystallization tendency. A vacuum atmosphere is beneficial for improving sintering rate and ultimate density, resulting in higher translucency than in an air atmosphere.
The sintering behavior of powder compacts of a boro - alumino - silicate glass was investigated under isothermal condition. In particular, the effect of sintering temperature, time and atmosphere on densification is systematically evaluated. Our sintering tests demonstrate that the densification can be significantly enhanced with increasing temperature, but relatively high translucency can be obtained in the temperature range in which there is a low crystallization tendency. In addition, a vacuum atmosphere is essential to sintering rate and ultimate density, thus leading to higher translucency than that in air atmosphere. Furthermore, the increase in densification accounts for the improvement of vickers hardness. These results are very relevant for the design of transparent glasses with powder sintering method.

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