期刊
INORGANIC CHEMISTRY COMMUNICATIONS
卷 133, 期 -, 页码 -出版社
ELSEVIER
DOI: 10.1016/j.inoche.2021.108925
关键词
Decolorization; Magnetic nanoparticles; Pomegranate peel extract (PPE); Azo dyes; Chemometrics
资金
- department of organic chemistry, faculty of pharmaceutical chemistry, Tehran medical sciences, Islamic Azad University, Tehran, Iran
This study developed silicate coated magnetic nanoparticles functionalized by pomegranate peel extract for dye treatment. The nanocatalyst showed high decolorization efficiency (> 99%) towards methyl blue and methyl orange dyes, making it a green and effective material for degrading carcinogenic azo dyes in real water samples. Reusability experiments were conducted for 8 consecutive runs, demonstrating the potential practical application of the superparamagnetic nanocatalyst.
This study has focused on the development and application of silicate coated magnetic nanoparticles functionalized by Pomegranate peel extract (PPE). Fe3O4 nanoparticles fabricated through the co-precipitation method and coating with silica then mixing with pomegranate peel extract. Afterward, Fe3O4@SiO2-PPE NPs were characterized by FT-IR, SEM, XRD and TEM. The obtained Fe3O4@SiO2-PPE nanostructure combined with H2O2 were employed as Fenton- like nanocatalyst in dye treatment processes. The effects of several factors including nanocatalyst amount, time period, temperature and H2O2 amount were measured simultaneously using chemometrics techniques. The Box-Behnken design (BBD) and response surface methodology (RSM) were used to explore the optimum conditions providing the highest decolorization efficiency. Under the optimum conditions, the decolorization efficiency toward methyl blue and methyl orange dyes were obtained > 99%. The obtained results indicated that the superparamagnetic nanocatalyst could be applied as a green and highly effective material for the degradation and decolorization of different carcinogenic azo dyes in real water samples. Reusability experiments has been performed for 8 consecutive runs.
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