期刊
CERAMICS INTERNATIONAL
卷 47, 期 21, 页码 29670-29680出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2021.07.138
关键词
Ablation evolution behavior; Millisecond laser; Micro-hole; Recast layer
资金
- Natural Science Foundation of Tianjin [18JCQNJC75600]
- National Key Research and Development Program of China [2019YFB1704802]
- Tianjin Research Innovation Project for Postgraduate Students [2020YJSS053]
- National Natural Sci-ence Foundation of China [51705362]
This paper investigates the ablation evolution behavior of 2.5D Cf/SiC composites, observing the ablation evolution process and recast layer structures at different fiber angles through millisecond laser processing. The study reveals the different stages of ablation evolution experienced by fibers and the diversity of recast layer structures.
2.5D Cf/SiC composite has been a key heat-resistant ceramic matrix composite (CMC) in aerospace field due to the special structure characteristics. Against the existing research almost focus on 'ablation behavior' in laser processing of CMC, this paper put forward the 'ablation evolution behavior' for the first time, and reveals the 'ablation evolution behavior' in micro-hole machining of 2.5D Cf/SiC composites with millisecond laser. The results show that 0 degrees fiber experiences the ablation evolution from filiform connection, flat ellipse, needle-like to convex structure. And the 90 degrees fiber suffers the ablation evolution from cylindrical structure, lotus lead shape, bud-shape to closed shape. The core of the 90 degrees fibers undergoes the topography structures from cylindrical protrusion, spherical protrusion to needle-like. Except for the honeycomb structure studied in existing research, four new recast layer structures, named transverse strip, longitudinal strip, shell structure, and multi-layer structure are found and analyzed. Further, the mechanism analysis reveals that the recast layer contains both oxidized characteristics and highly carbonized characteristics. In addition, the microstructural analysis shows that three types of particle topography adhere to the recast layer, that are spherical micro-protrusion (20-48 mu m), bubble particles (5-15 mu m), and sub-micron particles (<1 mu m).
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