期刊
GREEN CHEMISTRY
卷 18, 期 18, 页码 4879-4883出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6gc01196a
关键词
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资金
- National Natural Science Foundation of China [21302048]
- Hunan Provincial Natural Science Foundation of China [14JJ7028, 2016JJ4035]
- Scientific Research Hunan Provincial Education Department [15B095]
- Science and Technology Innovative Research Team in Higher Educational Institutions of Hunan Province [2012-318]
- Construct Program of the Key Discipline in Hunan Province
With water as the reaction medium, an efficient protocol has been developed for the synthesis of Z-beta-sulfonyl-alpha,beta-unsaturated carbonyl products via water-promoted sulfonylation of alkynylcarbonyl compounds with sodium sulfinates. This strategy could effectively avoid the use of toxic organic solvents, catalysts and additives. This method features a wide substrate scope with a broad range of functional group tolerance, utilizes easily available starting materials, can be scaled-up, and is operationally simple.
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