4.7 Article

Microstructure evolution and mechanical performance of ternary Zn-0.8Mg-0.2Sr (wt. %) alloy processed by equal-channel angular pressing

出版社

ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2021.141809

关键词

ECAP; Biodegradable zinc alloys; Strain hardening; Texture; Microstructure

资金

  1. Czech Science Foundation [18-06110 S]
  2. Operational Programme Research, Development and Education - European Structural and Investment Funds
  3. Czech Ministry of Education, Youth and Sports [SOLID21 - CZ.02.1.01/0.0/16 019/0000760]
  4. MEYS CR [LM2018110]

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The study reveals that continuous dynamic recrystallization is the main mechanism during the processing of Zn-0.8Mg-0.2Sr alloy, influencing grain size, residual stresses, and dislocation arrangement. The compressive tests show that the mechanical properties of the material are almost isotropic in individual directions, meeting the basic requirements for applications in implantology.
In this study, we prepared a Zn-0.8Mg-0.2Sr (wt. %) alloy and processed it by ECAP. The evolution of the microstructure during the processing was observed and discussed in detail. The obtained results revealed the continuous dynamic recrystallization as the prevailing recrystallization mechanism. It affected all the aspects of the microstructure, namely the grain size, residual stresses, and dislocation arrangement. The obtained grain size was in good agreement with both empirical and theoretical relations predicting the minimal (0.4-0.6 mu m) and average (2.5 mu m) grain size. The compressive tests revealed the relations between alignment of the intermetallic regions, texture of the Zn matrix, and resulting mechanical performance of the material. The compressive yield strength of the material ranged from 230 to 250 MPa in the individual directions, and the tensile yield strength reached the value of approximately 200 MPa. The resulting mechanical properties were almost isotropic in the individual directions and fulfilled the basic requirements for applications in implantology, particularly, for maxillofacial, cranial or orthopaedic implants.

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