4.7 Article

In situ high-energy X-ray study of deformation mechanisms in additively manufactured 316L stainless steel

期刊

JOURNAL OF NUCLEAR MATERIALS
卷 549, 期 -, 页码 -

出版社

ELSEVIER
DOI: 10.1016/j.jnucmat.2021.152874

关键词

316 stainless steel; Additive manufacturing; In situ X-ray diffraction; X-ray tomography; Tensile deformation

资金

  1. Transformational Challenge Reactor Program - U.S. Department of Energy, Office of Nuclear Energy [DE-AC02-06CH11357]
  2. DOE Office of Science [DE-AC02-06CH11357]

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The room-temperature tensile behavior of AM 316L SS was studied using high-energy X-ray diffraction and X-ray tomography. It was found that AM 316L SS exhibited high dislocation storage capability and an attractive combination of strength and ductility during plastic deformation. The morphological changes of built-in pores in AM 316L SS during deformation and fracture were also revealed to have significant roles in the material's performance.
A key structural material planned to be used in the core of the Transformational Challenge Reactor is the additively manufactured 316L stainless steel (AM 316L SS). While the deformation of conventionally-manufactured 316 SS have been extensively studied, the deformation mechanism of AM 316L SS is less known. Here the room-temperature tensile behavior of AM 316L SS was studied in situ using high-energy X-ray diffraction and X-ray tomography. Diffraction yielded the lattice strains and the dislocation densi-ties of the AM 316L SS, which were compared to those of a conventionally processed 316H SS. It was found that while the conventional 316H SS had three distinct deformation stages, namely stage II ather-mal hardening, stage III dynamic recovery, and stage IV, the AM 316L experienced only the stages III and IV after an initial transitional period. The plastic instability stresses (PIS), i.e. the true ultimate tensile strength, were nearly the same in both materials. The AM 316L had very low dislocation barrier strength throughout the plastic deformation, which, in combination with the invariant PIS, explained its high dis-location storage capability and the attractive combination of strength and ductility. Tomography revealed morphological changes of the built-in pores in the AM 316L during deformation and fracture, and it was concluded that large pores close to the surface might have significant roles in the necking stage. ? 2021 Elsevier B.V. All rights reserved.

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